4-BroMo-1-ethoxy-2-Methylbenzene

Base Information

• Chemical Name: 4-BroMo-1-ethoxy-2-Methylbenzene
• CAS No.: 79636-93-4
• Molecular Formula: C9H11BrO
• Molecular Weight: 215.08700
• Mol file: 79636-93-4.mol

Synonyms:4'-bromotrichloroacetanilide;4-bromo-1-ethoxy-2-methyl-benzene;4-bromo-N-trichloroacetylphenylamine;4-Brom-2-methyl-phenetol;4-bromo-2-methyl-phenetole;4-bromo-o-cresol ethyl ether;5-Brom-2-aethoxy-toluol;

Chemical Property of 4-BroMo-1-ethoxy-2-Methylbenzene

Chemical Property:

• PSA: 9.23000
• LogP: 3.15620
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

4-bromo-1-ethoxy-2-methylbenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-BroMo-1-ethoxy-2-Methylbenzene

There total 1 articles about 4-BroMo-1-ethoxy-2-Methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

4-Bromo-2-methylphenol (2362-12-1) + ethyl iodide (75-03-6) → 4-bromo-1-ethoxy-2-methylbenzene (79636-93-4)

Guidance literature:

4-Bromo-2-methylphenol; With potassium carbonate; In dimethyl sulfoxide; at 20 ℃;

ethyl iodide; In dimethyl sulfoxide; at 60 ℃;

Reference yield: 73.0%

4-bromo-1-ethoxy-2-methylbenzene (79636-93-4) + ethylene glycol (107-21-1) → 2-(4-ethoxy-3-methylphenyl)-1,3,2-dioxaborolane (1310403-97-4)

Guidance literature:

4-bromo-1-ethoxy-2-methylbenzene; With magnesium; In tetrahydrofuran;

With Trimethyl borate; In tetrahydrofuran; at -78 - 20 ℃;

ethylene glycol; In toluene; Reflux;

DOI:10.1002/ejoc.201403214

Reference yield: 50.0%

4-bromo-1-ethoxy-2-methylbenzene (79636-93-4) → 5-bromo-2-ethoxybenzaldehyde (79636-94-5)

Guidance literature:

With pyridine; dipotassium peroxodisulfate; copper(I) sulfate; In water; acetonitrile; at 65 - 70 ℃; for 3h;

DOI:10.1016/S0040-4039(01)90532-5

upstream raw materials:

4-Bromo-2-methylphenol

ethyl iodide

Downstream raw materials:

5-bromo-2-ethoxybenzaldehyde

C₁₇H₁₉BrO₂

1-(5-bromo-2-ethoxyphenyl)cyclopropanecarbonitrile

4-bromo-2-(bromomethyl)-1-ethoxybenzene

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