N-tert-Butyldibenzylamine

Base Information

• Chemical Name: N-tert-Butyldibenzylamine
• CAS No.: 30923-82-1
• Molecular Formula: C18H23 N
• Molecular Weight: 253.387
• Hs Code.: 2921499090
• European Community (EC) Number: 250-389-8
• NSC Number: 151990
• DSSTox Substance ID: DTXSID00184915
• Nikkaji Number: J287.410E
• Wikidata: Q83055854
• Mol file: 30923-82-1.mol

Synonyms:N-tert-Butyldibenzylamine;30923-82-1;N,N-dibenzyl-2-methylpropan-2-amine;Benzenemethanamine, N-(1,1-dimethylethyl)-N-(phenylmethyl)-;DIBENZYL(TERT-BUTYL)AMINE;EINECS 250-389-8;N,N-Dibenzyl-t-butylamine;t-butyldibenzylamine;NSC151990;SCHEMBL5962473;DTXSID00184915;ADAL1056269;N(Cc1ccccc1)(Cc2ccccc2)C(C)(C)C;NSC 151990;NSC-151990;N,N-Dibenzyl-2-methyl-2-propanamine #;E83741

Chemical Property of N-tert-Butyldibenzylamine

Chemical Property:

• Vapor Pressure: 0.000183mmHg at 25°C
• Melting Point: 68-70 °C
• Boiling Point: 329°Cat760mmHg
• PKA: 8.09±0.50(Predicted)
• Flash Point: 138.8°C
• PSA: 3.24000
• Density: 0.988g/cm³
• LogP: 4.48730
• XLogP3: 4.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 5
• Exact Mass: 253.183049738
• Heavy Atom Count: 19
• Complexity: 221

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)(C)N(CC1=CC=CC=C1)CC2=CC=CC=C2

Technology Process of N-tert-Butyldibenzylamine

There total 18 articles about N-tert-Butyldibenzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N,N-dibenzyl-O-benzoylhydroxylamine (52742-32-2) + di-tert-butylzinc (16636-96-7) → N,N-dibenzyl-2-methylpropan-2-amine (30923-82-1)

Guidance literature:

With copper(I) trifluoromethanesulfonate benzene; In tetrahydrofuran; at 25 ℃; for 1h;

DOI:10.1021/ja049474e

Reference yield: 89.0%

N,N-dibenzyl-O-benzoylhydroxylamine (52742-32-2) + tert-butylmagnesium chloride (677-22-5) → N,N-dibenzyl-2-methylpropan-2-amine (30923-82-1)

Guidance literature:

With copper dichloride; In tetrahydrofuran; at 20 ℃; for 0.25h;

DOI:10.1021/ol0702829

Reference yield: 30.0%

benzyl bromide (100-39-0) + tert-butylamine (75-64-9) → N,N-dibenzyl-2-methylpropan-2-amine (30923-82-1) + N-tert-butylbenzylamine (3378-72-1)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 16h;

DOI:10.1039/b006852g

upstream raw materials:

benzyl chloride

N-tert-butylbenzylamine

N,N-Dibenzyl-2-chloro-2-methyl-propionamide

tert-butylamine

Downstream raw materials:

N-benzyl-N-(tert-butyl)nitrous amide

N-tert-butylbenzylamine