Benzenamine, 4-bromo-N-(1-phenylethylidene)-

Base Information

Chemical Name:Benzenamine, 4-bromo-N-(1-phenylethylidene)-
CAS No.:80070-91-3
Molecular Formula:C₁₄H₁₂BrN
Molecular Weight:274.16
Hs Code.:
DSSTox Substance ID:DTXSID10469841
Nikkaji Number:J1.956.665J

Synonyms:Benzenamine, 4-bromo-N-(1-phenylethylidene)-;80070-91-3;SCHEMBL15137057;SCHEMBL15137058;DTXSID10469841

Suppliers and Price of Benzenamine, 4-bromo-N-(1-phenylethylidene)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenamine, 4-bromo-N-(1-phenylethylidene)-

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:273.01531
Heavy Atom Count:16
Complexity:235

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NC1=CC=C(C=C1)Br)C2=CC=CC=C2

Technology Process of Benzenamine, 4-bromo-N-(1-phenylethylidene)-

There total 8 articles about Benzenamine, 4-bromo-N-(1-phenylethylidene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 536-74-3
phenylacetylene

: 106-40-1
4-bromo-aniline

: 125231-24-5,80070-91-3
4-bromo-N-(α-methylbenzylidene)aniline

Guidance literature:: With Cu-exchanged tungstophosphoric acid; at 80 ℃; for 2h; regioselective reaction; neat (no solvent);
DOI:10.1016/j.tetlet.2008.10.131

Reference yield: 66.0%

: 98-86-2
acetophenone

: 106-40-1
4-bromo-aniline

: 125231-24-5,80070-91-3
4-bromo-N-(α-methylbenzylidene)aniline

Guidance literature:: With Hβ zeolite; In toluene; at 120 ℃; for 24h; Sealed tube; Green chemistry;
DOI:10.1007/s10562-017-2196-0

Reference yield: 5.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 106-40-1
4-bromo-aniline

: 125231-24-5,80070-91-3
4-bromo-N-(α-methylbenzylidene)aniline

Guidance literature:: With pyridine; oxygen; palladium diacetate; In neat (no solvent); regioselective reaction; Molecular sieve; Heating;
DOI:10.1021/acs.orglett.7b02532