N-Isoamylphthalamide

Base Information

Chemical Name:N-Isoamylphthalamide
CAS No.:41764-14-1
Molecular Formula:C13H15 N O2
Molecular Weight:217.268
Hs Code.:
NSC Number:68528
DSSTox Substance ID:DTXSID90194588
Nikkaji Number:J561.533J
Wikidata:Q83067368
Mol file:41764-14-1.mol

Synonyms:N-isoamylphthalamide

Suppliers and Price of N-Isoamylphthalamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of N-Isoamylphthalamide

Chemical Property:

Vapor Pressure:0.000358mmHg at 25°C
Boiling Point:318.6°Cat760mmHg
Flash Point:131°C
PSA：37.38000
Density:1.143g/cm³
LogP:2.26660
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:217.110278721
Heavy Atom Count:16
Complexity:274

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)CCN1C(=O)C2=CC=CC=C2C1=O

Technology Process of N-Isoamylphthalamide

There total 3 articles about N-Isoamylphthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 85-44-9
phthalic anhydride

: 55210-77-0
1-azido-3-methylbutane

: 41764-14-1
2-(3-methylbutyl)-2,3-dihydro-1H-isoindole-1,3-dione

Guidance literature:: With triphenylphosphine; tetra-n-butylammonium cyanide; In benzene; for 12h; Ambient temperature;
DOI:10.1016/S0040-4039(00)84061-7

Reference yield: 85.0%

: 85-44-9
phthalic anhydride

: 107-85-7
1-amino-3-methylbutane

: 41764-14-1
2-(3-methylbutyl)-2,3-dihydro-1H-isoindole-1,3-dione

Guidance literature:: at 120 ℃; for 2h; Sealed tube;
DOI:10.1021/acs.orglett.1c03087

Reference yield:

: 20213-82-5
2-(3-methyl-but-3-enyl)-2,3-dihydro-1H-isoindole-1,3-dione

: 74-88-4
methyl iodide

: 15818-31-2
2-(3,3-dimethylbutyl)isoindoline-1,3-dione

: 1026984-09-7
2-(3-methyl-pentyl)-isoindole-1,3-dione

: 41764-14-1
2-(3-methylbutyl)-2,3-dihydro-1H-isoindole-1,3-dione

Guidance literature:: With bis(acetylacetonate)nickel(II); manganese(III) (Z)-2,2,6,6-tetramethyl-5-oxohept-3-en-3-olate; 1,1,1,3',3',3'-hexafluoro-propanol; phenylsilane; potassium carbonate; In 1,2-dichloro-ethane; at 0 - 20 ℃; for 30h; Overall yield = 64 %Spectr.; Sealed tube;
DOI:10.1021/jacs.9b02844 DOI:10.1021/jacs.9b02844