2-[(2-Methylphenyl)sulfanyl]pyridine

Base Information

Chemical Name:2-[(2-Methylphenyl)sulfanyl]pyridine
CAS No.:81994-64-1
Molecular Formula:C12H11NS
Molecular Weight:201.292
Hs Code.:
DSSTox Substance ID:DTXSID40525686
Nikkaji Number:J2.713.615J
Wikidata:Q82393465

Synonyms:81994-64-1;2-[(2-Methylphenyl)sulfanyl]pyridine;SCHEMBL4439023;DTXSID40525686

Suppliers and Price of 2-[(2-Methylphenyl)sulfanyl]pyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-[(2-Methylphenyl)sulfanyl]pyridine

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:201.06122053
Heavy Atom Count:14
Complexity:172

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=CC=C1SC2=CC=CC=N2

Technology Process of 2-[(2-Methylphenyl)sulfanyl]pyridine

There total 4 articles about 2-[(2-Methylphenyl)sulfanyl]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 109-09-1
2-chloropyridine

: 137-06-4
2-thiocresol

: 81994-64-1
2-[(2-methylphenyl)thio]pyridine

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; bis(η3-allyl-μ-chloropalladium(II)); sodium t-butanolate; In toluene; at 120 ℃; for 17h;
DOI:10.1016/j.catcom.2018.03.025

Reference yield: 75.0%

: 57785-86-1
pyridin-2-yl tosylate

: 137-06-4
2-thiocresol

: 81994-64-1
2-[(2-methylphenyl)thio]pyridine

Guidance literature:: With C₂₃H₂₄ClNiP; lithium tert-butoxide; In N,N-dimethyl-formamide; at 100 ℃; for 6h; Reagent/catalyst; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.202101906

Reference yield:

: 87641-74-5
2,2,4,4-tetrachloro-2,4-dihydro-1,3-benzodithiin

: 81994-64-1
2-[(2-methylphenyl)thio]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminum hydride / tetrahydrofuran / 7 h / Heating

2: 1.) NaOH / 1.) N,N-dimeemthylacetamide, 150 deg C; 2.) heating, overnight

With sodium hydroxide; lithium aluminium tetrahydride; In tetrahydrofuran;