Triphenyl[1-(trimethylsilyl)propylidene]-lambda~5~-phosphane

Base Information

Chemical Name:Triphenyl[1-(trimethylsilyl)propylidene]-lambda~5~-phosphane
CAS No.:82294-34-6
Molecular Formula:C24H29PSi
Molecular Weight:376.554
Hs Code.:
DSSTox Substance ID:DTXSID90509335
Nikkaji Number:J505.432J
Wikidata:Q82366814

Synonyms:82294-34-6;DTXSID90509335;Triphenyl[1-(trimethylsilyl)propylidene]-lambda~5~-phosphane

Suppliers and Price of Triphenyl[1-(trimethylsilyl)propylidene]-lambda~5~-phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Triphenyl[1-(trimethylsilyl)propylidene]-lambda~5~-phosphane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:5
Exact Mass:376.17761446
Heavy Atom Count:26
Complexity:431

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(=P(C1=CC=CC=C1)(C2=CC=CC=C2)C3=CC=CC=C3)[Si](C)(C)C

Technology Process of Triphenyl[1-(trimethylsilyl)propylidene]-lambda~5~-phosphane

There total 5 articles about Triphenyl[1-(trimethylsilyl)propylidene]-lambda~5~-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 144189-83-3
Triphenyl-(1-trimethylsilanyl-propyl)-phosphonium; iodide

: 82294-34-6
1-trimethylsilyl propylidene triphenylphosphorane

Guidance literature:: With sodium hexamethyldisilazane; In diethyl ether; for 20h; Ambient temperature;
DOI:10.1055/s-1992-26227

Reference yield: 85.0%

: 75-77-4
chloro-trimethyl-silane

: 16666-78-7
propylidenetriphenylphosphorane

: 82294-34-6
1-trimethylsilyl propylidene triphenylphosphorane

Guidance literature:: In benzene; at 80 ℃; for 20h;
DOI:10.1055/s-1992-26227

Reference yield:

: 16666-78-7
propylidenetriphenylphosphorane

: 82294-34-6
1-trimethylsilyl propylidene triphenylphosphorane

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / toluene / a) -78 deg C, b) r.t., 15-20 h

2: 89 percent / Na3)2> / diethyl ether / 20 h / Ambient temperature

With sodium hexamethyldisilazane; In diethyl ether; toluene;
DOI:10.1055/s-1992-26227