2-hydroxy-1,2,3,3-tetraphenylpropan-1-one

Base Information

• Chemical Name: 2-hydroxy-1,2,3,3-tetraphenylpropan-1-one
• CAS No.: 7474-66-0
• Molecular Formula: C27H22 O2
• Molecular Weight: 378.47

Synonyms:Propiophenone, 2-hydroxy-2,3,3-triphenyl- (6CI); Propiophenone, a-hydroxy-a,b,b-triphenyl- (3CI); NSC 401882; NSC 401894

Chemical Property of 2-hydroxy-1,2,3,3-tetraphenylpropan-1-one

Chemical Property:

• Vapor Pressure: 1.04E-12mmHg at 25°C
• Boiling Point: 545°Cat760mmHg
• Flash Point: 229.5°C
• Density: 1.178g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-hydroxy-1,2,3,3-tetraphenylpropan-1-one

There total 4 articles about 2-hydroxy-1,2,3,3-tetraphenylpropan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

α-benzhydryloxy-deoxybenzoin (213617-90-4) → 1,1-Diphenylmethanol (91-01-0) + 2,2-diphenylacetic acid (117-34-0) + 2-hydroxy-1,2,3,3-tetraphenyl-propan-1-one (7474-66-0) + 1-hydroxy-1,1,3,3-tetraphenyl-acetone (7476-10-0)

Guidance literature:

Produkt 5: 1,1,2,2-Tetraphenyl-aethan; Produkt 6: Benzoesaeure;

DOI:10.1021/ja01150a062

Reference yield:

1,1-Diphenylmethanol (91-01-0) + 2-hydroxy-2-phenylacetophenone (119-53-9,579-44-2) → 2-hydroxy-1,2,3,3-tetraphenyl-propan-1-one (7474-66-0)

Guidance literature:

With toluene-4-sulfonic acid; benzene; unter Entfernen des entstehenden Wassers;

DOI:10.1021/ja01150a062

Reference yield:

phenylmagnesium bromide → 1,2,3,3-tetraphenylprop-2-en-1-one (6333-11-5) + 2-hydroxy-1,2,3,3-tetraphenyl-propan-1-one (7474-66-0)

Guidance literature:

With diethyl ether; und Leiten von trockenem Sauerstoff durch das Reaktionsgemisch;

DOI:10.1021/ja01351a025

upstream raw materials:

1,1-Diphenylmethanol

2-hydroxy-2-phenylacetophenone

(E)-2-phenylchalcone

α-benzhydryloxy-deoxybenzoin

Downstream raw materials:

benzophenone

benzil

1,2,2-triphenylethan-1-one

benzoic acid

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