Silane, (1,1-dimethylethyl)(5-ethenyl-2-methoxyphenoxy)dimethyl-

Base Information

Chemical Name:Silane, (1,1-dimethylethyl)(5-ethenyl-2-methoxyphenoxy)dimethyl-
CAS No.:831222-65-2
Molecular Formula:C15H24O2Si
Molecular Weight:264.44
Hs Code.:
DSSTox Substance ID:DTXSID40466247
Wikidata:Q82292772

Synonyms:831222-65-2;Silane, (1,1-dimethylethyl)(5-ethenyl-2-methoxyphenoxy)dimethyl-;DTXSID40466247;EN300-45209106;TERT-BUTYL(5-ETHENYL-2-METHOXYPHENOXY)DIMETHYLSILANE

Suppliers and Price of Silane, (1,1-dimethylethyl)(5-ethenyl-2-methoxyphenoxy)dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Silane, (1,1-dimethylethyl)(5-ethenyl-2-methoxyphenoxy)dimethyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:264.154556538
Heavy Atom Count:18
Complexity:281

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)[Si](C)(C)OC1=C(C=CC(=C1)C=C)OC

Technology Process of Silane, (1,1-dimethylethyl)(5-ethenyl-2-methoxyphenoxy)dimethyl-

There total 4 articles about Silane, (1,1-dimethylethyl)(5-ethenyl-2-methoxyphenoxy)dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 863479-34-9
3-(tert-butyldimethylsiloxy)-4-methoxyphenylacetylene

: 831222-65-2
tert-butyl-(2-methoxy-5-vinylphenoxy)dimethylsilane

Guidance literature:: With dimethylamine borane; In ethanol; at 25 ℃; for 0.8h; Reagent/catalyst; Time;
DOI:10.1039/c4cc08163c

Reference yield: 78.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 97315-18-9
p-methoxy-m-(tert-butyldimethylsilyloxy)-benzaldehyde

: 831222-65-2
tert-butyl-(2-methoxy-5-vinylphenoxy)dimethylsilane

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 5h;
DOI:10.1016/j.tetlet.2008.01.135

Reference yield:

: 621-59-0
isovanillin

: 831222-65-2
tert-butyl-(2-methoxy-5-vinylphenoxy)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: imidazole / CH₂Cl₂ / 0 - 20 °C

2.1: n-butyl lithium / tetrahydrofuran / 0.25 h

2.2: tetrahydrofuran

With 1H-imidazole; n-butyllithium; In tetrahydrofuran; dichloromethane; 2.2: Wittig olefination;
DOI:10.1021/ol0705907