Stannane, (1-methylethylidene)bis[chlorodimethyl-

Base Information

Chemical Name:Stannane, (1-methylethylidene)bis[chlorodimethyl-
CAS No.:83135-44-8
Molecular Formula:C7H18Cl2Sn2
Molecular Weight:410.546
Hs Code.:
DSSTox Substance ID:DTXSID30411822

Synonyms:Stannane, (1-methylethylidene)bis[chlorodimethyl-;83135-44-8;DTXSID30411822

Suppliers and Price of Stannane, (1-methylethylidene)bis[chlorodimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Stannane, (1-methylethylidene)bis[chlorodimethyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:409.88237
Heavy Atom Count:11
Complexity:137

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)([Sn](C)(C)Cl)[Sn](C)(C)Cl

Technology Process of Stannane, (1-methylethylidene)bis[chlorodimethyl-

There total 1 articles about Stannane, (1-methylethylidene)bis[chlorodimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 83135-43-7
2,2-bis(trimethylstannyl)propane

: 753-73-1
dimethyltin dichloride

: 83135-44-8
2,2-bis(chlorodimethylstannyl)propane

: 1066-45-1
trimethyltin(IV)chloride

Guidance literature:: In neat (no solvent); 2,2-bis(trimethylstannyl)propane placed in flash with 2 mol of dimethyldichlorostannane, heated at 60°C overnight; stirred at 15-20 Torr, warmed at 0.01 Torr to 100°C, recrystd. (CCl4); elem. anal.;
DOI:10.1021/om00073a020

Reference yield: 75.0%

: 83135-44-8
2,2-bis(chlorodimethylstannyl)propane

: 7646-78-8
tin(IV) chloride

: 83135-45-9
2-(chlorodimethylstannyl)-2-(dichloromethylstannyl)propane

: 753-73-1
dimethyltin dichloride

Guidance literature:: In dichloromethane; 1 mol of 2,2-bis(dimethylchlorostannyl)propane, CH2Cl2 and 0.5 mol of tetrachlorostannane placed into flask, warmed and solvent removed (vac.),warmed to 60°C overnight; stirred at 60°C under 0.01 Torr, recrystd. (petroleum ether); elem. anal.;
DOI:10.1021/om00073a020

Reference yield: 70.0%

: 83135-44-8
2,2-bis(chlorodimethylstannyl)propane

: 7646-78-8
tin(IV) chloride

: 83135-46-0
(CH₃Cl₂Sn)2C(CH₃)2

: 1066-45-1
trimethyltin(IV)chloride

: 753-73-1
dimethyltin dichloride

Guidance literature:: In dichloromethane; CH2Cl2 added to 2,2-bis(dimethylchlorostannyl)propane, excess of SnCl4 added slowly, agitated for 5 min, concd. (vac.), heated at 60°C overnight; warmed to 60°C for 0.5 h with slow reducing pressure to 0.01 Torr, recrystd. (CCl4); elem. anal.;
DOI:10.1021/om00073a020