Benzoic acid, 3-fluoro-4-methoxy-5-(phenylmethoxy)-, methyl ester

Base Information

Chemical Name:Benzoic acid, 3-fluoro-4-methoxy-5-(phenylmethoxy)-, methyl ester
CAS No.:838856-89-6
Molecular Formula:C16H15FO4
Molecular Weight:290.291
Hs Code.:

Synonyms:

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Chemical Property of Benzoic acid, 3-fluoro-4-methoxy-5-(phenylmethoxy)-, methyl ester

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Technology Process of Benzoic acid, 3-fluoro-4-methoxy-5-(phenylmethoxy)-, methyl ester

There total 6 articles about Benzoic acid, 3-fluoro-4-methoxy-5-(phenylmethoxy)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 838856-88-5
3-fluoro-5-hydroxy-4-methoxybenzoic acid methyl ester

: 100-39-0
benzyl bromide

: 838856-89-6
methyl 3-fluoro-4-(methyloxy)-5-[(phenylmethyl)oxy]benzoate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

Reference yield:

: 838856-86-3
methyl 3-(acetyloxy)-4-(methyloxy)-5-nitrobenzoate

: 838856-89-6
methyl 3-fluoro-4-(methyloxy)-5-[(phenylmethyl)oxy]benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 24 h / 760.05 Torr

2.1: boron trifluoride diethyl etherate / 1,2-dimethoxyethane / 0.02 - 0.03 h / 0 °C

2.2: 0.25 h / 0 °C

3.1: 1,2,4-Trichlorobenzene / 17 h / 110 °C

4.1: caesium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

With boron trifluoride diethyl etherate; hydrogen; caesium carbonate; palladium 10% on activated carbon; In 1,2-dimethoxyethane; ethyl acetate; N,N-dimethyl-formamide; 1,2,4-Trichlorobenzene;

Reference yield:

: 6702-50-7
3-hydroxy-4-methoxybenzoate

: 838856-89-6
methyl 3-fluoro-4-(methyloxy)-5-[(phenylmethyl)oxy]benzoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium acetate / 20 h / 20 °C

2.1: sulfuric acid; nitric acid / water / 0.42 h / -5 °C

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 24 h / 760.05 Torr

4.1: boron trifluoride diethyl etherate / 1,2-dimethoxyethane / 0.02 - 0.03 h / 0 °C

4.2: 0.25 h / 0 °C

5.1: 1,2,4-Trichlorobenzene / 17 h / 110 °C

6.1: caesium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

With sulfuric acid; boron trifluoride diethyl etherate; hydrogen; nitric acid; sodium acetate; caesium carbonate; palladium 10% on activated carbon; In 1,2-dimethoxyethane; water; ethyl acetate; N,N-dimethyl-formamide; 1,2,4-Trichlorobenzene;