2-Hydroxy-3,5-dimethoxy-4-methylbenzaldehyde

Base Information

Chemical Name:2-Hydroxy-3,5-dimethoxy-4-methylbenzaldehyde
CAS No.:85071-58-5
Molecular Formula:C10H12O4
Molecular Weight:196.203
Hs Code.:
DSSTox Substance ID:DTXSID10428271
Wikidata:Q82241084

Synonyms:2-hydroxy-3,5-dimethoxy-4-methylbenzaldehyde;85071-58-5;2-Hydroxy-3,5-dimethoxy-4-methyl-benzaldehyde;SCHEMBL5144957;DTXSID10428271;AKOS006229730

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Hydroxy-3,5-dimethoxy-4-methylbenzaldehyde

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:196.07355886
Heavy Atom Count:14
Complexity:195

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C=C(C(=C1OC)O)C=O)OC

Technology Process of 2-Hydroxy-3,5-dimethoxy-4-methylbenzaldehyde

There total 5 articles about 2-Hydroxy-3,5-dimethoxy-4-methylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 19676-67-6
2,4-dimethoxy-3-methylphenol

: 100-97-0
hexamethylenetetramine

: 85071-58-5
2-hydroxy-3,5-dimethoxy-4-methylbenzaldehyde

Guidance literature:: With trifluoroacetic acid; trifluoroacetic anhydride; at 0 ℃; for 45h; Heating / reflux;

Reference yield:

: 7149-92-0
2,4-dimethoxy-3-methylbenzaldehyde

: 85071-58-5
2-hydroxy-3,5-dimethoxy-4-methylbenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: m-CPBA; TsOH / CH₂Cl₂ / 20 °C

2: K₂CO₃ / CH₂Cl₂; methanol

3: 60 percent / acetic acid / Heating

With potassium carbonate; toluene-4-sulfonic acid; acetic acid; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; 1: Baeyer-Villiger oxidation / 3: Duff ortho-formylation;
DOI:10.1021/ja060369+

Reference yield:

: 5673-07-4
2,6-dimethoxytoluene

: 85071-58-5
2-hydroxy-3,5-dimethoxy-4-methylbenzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / TiCl₄

2: m-CPBA; TsOH / CH₂Cl₂ / 20 °C

3: K₂CO₃ / CH₂Cl₂; methanol

4: 60 percent / acetic acid / Heating

With titanium tetrachloride; potassium carbonate; toluene-4-sulfonic acid; acetic acid; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; 2: Baeyer-Villiger oxidation / 4: Duff ortho-formylation;
DOI:10.1021/ja060369+