1,2-Di(pyrrolidin-1-yl)ethane-1,2-dione

Base Information

Chemical Name:1,2-Di(pyrrolidin-1-yl)ethane-1,2-dione
CAS No.:85802-71-7
Molecular Formula:C10H16N2O2
Molecular Weight:196.249
Hs Code.:
DSSTox Substance ID:DTXSID70398522
Nikkaji Number:J1.921.918F
Wikidata:Q82200556

Synonyms:STK024744;85802-71-7;1,2-di(pyrrolidin-1-yl)ethane-1,2-dione;SCHEMBL8288869;DTXSID70398522;1,2-Dipyrrolizino-1,2-ethanedione;AKOS005379545

Suppliers and Price of 1,2-Di(pyrrolidin-1-yl)ethane-1,2-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Di(pyrrolidin-1-yl)ethane-1,2-dione

Chemical Property:

XLogP3:0.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:196.121177757
Heavy Atom Count:14
Complexity:215

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCN(C1)C(=O)C(=O)N2CCCC2

Technology Process of 1,2-Di(pyrrolidin-1-yl)ethane-1,2-dione

There total 4 articles about 1,2-Di(pyrrolidin-1-yl)ethane-1,2-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 123-75-1
pyrrolidine

: 201230-82-2
carbon monoxide

: 31268-20-9
bromomethyl phenyl sulfoxide

: 85802-71-7
1,2-dioxo-1,2-di(pyrrolidin-1-yl)ethane

: 120173-05-9
2-(phenylsulfinyl)-1-(pyrrolidin-1-yl)ethanone

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; cesium fluoride; In tetrahydrofuran; at 65 ℃; under 760.051 Torr;
DOI:10.1021/jo301778n DOI:10.1021/jo301778n

Reference yield: 85.0%

: 123-75-1
pyrrolidine

: 88428-62-0
(((CH₂)4)NH)2NiBr₂

: 3760-54-1
1-pyrrolidinecarboxaldehyde

: 81759-25-3
1,1'-carbonyldipyrrolidine

: 55810-80-5
pyrrolidinium hydrobromide

: 85802-71-7
1,2-dioxo-1,2-di(pyrrolidin-1-yl)ethane

: 13463-39-3,71564-36-8
tetracarbonyl nickel

Guidance literature:: With carbon monoxide; In tetrahydrofuran; diethyl ether; reaction in THF/Et2O = 2/1 soln., room temp., under CO (1 bar);
DOI:10.1016/S0022-328X(00)99113-7