H-GLY-PHE-GLY-OH

Base Information

Chemical Name:H-GLY-PHE-GLY-OH
CAS No.:14656-09-8
Molecular Formula:C13H17N3O4
Molecular Weight:279.296
Hs Code.:2924299090
Mol file:14656-09-8.mol

Synonyms:GLYCYL-L-PHENYLALANYL-GLYCINE;H-GLY-PHE-GLY-OH

Suppliers and Price of H-GLY-PHE-GLY-OH

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
H-Gly-Phe-Gly-OH
10mg
$ 45.00

Total 19 raw suppliers

Chemical Property of H-GLY-PHE-GLY-OH

Chemical Property:

Vapor Pressure:2.45E-19mmHg at 25°C
Boiling Point:678.5°Cat760mmHg
Flash Point:364.1°C
PSA：121.52000
Density:1.296g/cm³
LogP:0.35550
Storage Temp.:-15°C

Purity/Quality:

99% ^*data from raw suppliers

H-Gly-Phe-Gly-OH ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of H-GLY-PHE-GLY-OH

There total 6 articles about H-GLY-PHE-GLY-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.7%

: Fmoc-gly-wang resin

: 29022-11-5
N-(fluoren-9-ylmethoxycarbonyl)glycine

: 35661-40-6
N-Fmoc L-Phe

: 14656-09-8
glycyl-L-phenylalanyl-glycine

Guidance literature:: Fmoc-gly-wang resin; With piperidine; In N,N-dimethyl-formamide; Wang resin

N-Fmoc L-Phe; With 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); diisopropylamine; ethyl cyanoglyoxylate-2-oxime; In N,N-dimethyl-formamide; for 0.75h; Wang resin

N-(fluoren-9-ylmethoxycarbonyl)glycine; Further stages;
DOI:10.1002/ejoc.201300340

Reference yield:

: 14656-09-8
glycyl-L-phenylalanyl-glycine

Guidance literature:: With acetic acid;
DOI:10.1021/ja01520a065 DOI:10.1021/ja01588a027

Reference yield:

: 2-chlorotrityl resin

: 29022-11-5
N-(fluoren-9-ylmethoxycarbonyl)glycine

: 35737-10-1
N-Fmoc-β-alanine

: 35661-40-6
N-Fmoc L-Phe

: 42538-54-5
Glyβ-AlaGly

: 14656-09-8
glycyl-L-phenylalanyl-glycine

Guidance literature:: 2-chlorotrityl resin; N-Fmoc-β-alanine; N-Fmoc L-Phe; With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

With piperidine; In N,N-dimethyl-formamide;

N-(fluoren-9-ylmethoxycarbonyl)glycine; Further stages;
DOI:10.1016/j.tetlet.2017.03.021