Benzaldehyde, 4-Methoxy-2-(1-Methylethoxy)-

Base Information

• Chemical Name: Benzaldehyde, 4-Methoxy-2-(1-Methylethoxy)-
• CAS No.: 107811-48-3
• Molecular Formula: C11H14 O3
• Molecular Weight: 194.23
• Mol file: 107811-48-3.mol

Synonyms:2-isopropoxy-4-methoxybenzaldehyde;2-isopropoxy-4-methoxybenzene-1-carboaldehyde;Benzaldehyde,4-methoxy-2-(1-methylethoxy);4-methoxy-2-(propan-2-yloxy)benzaldehyde;(4-Methyl-2-(1-methylethoxy)phenyl)methanone;

Chemical Property of Benzaldehyde, 4-Methoxy-2-(1-Methylethoxy)-

Chemical Property:

• Vapor Pressure: 0.000386mmHg at 25°C
• Boiling Point: 317.4°Cat760mmHg
• Flash Point: 136.7°C
• PSA: 35.53000
• Density: 1.064g/cm³
• LogP: 2.29490

Purity/Quality:

97% ^*data from raw suppliers

4-Methoxy-2-(propan-2-yloxy)benzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzaldehyde, 4-Methoxy-2-(1-Methylethoxy)-

There total 3 articles about Benzaldehyde, 4-Methoxy-2-(1-Methylethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-Hydroxy-4-methoxybenzaldehyde (673-22-3) + isopropyl bromide (75-26-3) → 2-isopropoxy-4-methoxybenzene-1-carboaldehyde (107811-48-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 40 ℃; for 5h; Inert atmosphere;

DOI:10.1016/j.bmc.2011.07.050

Reference yield: 90.0%

2-Hydroxy-4-methoxybenzaldehyde (673-22-3) + 2-iodo-propane (75-30-9) → 2-isopropoxy-4-methoxybenzene-1-carboaldehyde (107811-48-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; for 12h; Heating;

DOI:10.1021/ja0302228

Reference yield:

2,4-Dihydroxybenzaldehyde (95-01-2) → 2-isopropoxy-4-methoxybenzene-1-carboaldehyde (107811-48-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 3 h / Reflux

2: potassium carbonate / acetone / 5 h / 40 °C

With potassium carbonate; In acetone;

DOI:10.2174/1570180811666140116214111

upstream raw materials:

2-Hydroxy-4-methoxybenzaldehyde

isopropyl bromide

2-iodo-propane

2,4-Dihydroxybenzaldehyde

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