Phenyl 1-bromo-2-(ethylamino)ethane-1-sulfonate

Base Information

Chemical Name:Phenyl 1-bromo-2-(ethylamino)ethane-1-sulfonate
CAS No.:87975-09-5
Molecular Formula:C₁₀H₁₄BrNO₃S
Molecular Weight:308.196
Hs Code.:
DSSTox Substance ID:DTXSID70579394

Synonyms:87975-09-5;Phenyl 1-bromo-2-(ethylamino)ethane-1-sulfonate;DTXSID70579394

Suppliers and Price of Phenyl 1-bromo-2-(ethylamino)ethane-1-sulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Phenyl 1-bromo-2-(ethylamino)ethane-1-sulfonate

Chemical Property:

PSA：63.78000
LogP:3.19740
XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:306.98778
Heavy Atom Count:16
Complexity:283

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCNCC(S(=O)(=O)OC1=CC=CC=C1)Br

Technology Process of Phenyl 1-bromo-2-(ethylamino)ethane-1-sulfonate

There total 4 articles about Phenyl 1-bromo-2-(ethylamino)ethane-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 6904-89-8
Phenyl 1-bromoethenesulfonate

: 75-04-7,85404-22-4
ethylamine

: 87975-09-5
1-Bromo-2-ethylamino-ethanesulfonic acid phenyl ester

Guidance literature:: In benzene; for 24h; Ambient temperature;
DOI:10.1055/s-1983-30527

Reference yield: 64.0%

: 6855-00-1
Phenyl 1,2-dibromoethanesulfonate

: 75-04-7,85404-22-4
ethylamine

: 87975-09-5
1-Bromo-2-ethylamino-ethanesulfonic acid phenyl ester

Guidance literature:: In benzene; for 24h; Ambient temperature;
DOI:10.1055/s-1983-30527

Reference yield:

: 1562-34-1
phenyl vinylsulfonate

: 87975-09-5
1-Bromo-2-ethylamino-ethanesulfonic acid phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Br₂, azodiisobutyronitrile / CCl₄ / 1.) reflux, 4 h; 2,) room temp., 48 h

2: 80 percent / triethylamine / benzene / 24 h / Ambient temperature

3: 64 percent / benzene / 24 h / Ambient temperature

With 2,2'-azobis(isobutyronitrile); bromine; triethylamine; In tetrachloromethane; benzene;
DOI:10.1055/s-1983-30527