Phenyl 1-bromo-2-(cyclohexylamino)ethane-1-sulfonate

Base Information

Chemical Name:Phenyl 1-bromo-2-(cyclohexylamino)ethane-1-sulfonate
CAS No.:87975-12-0
Molecular Formula:C14H20BrNO3S
Molecular Weight:362.288
Hs Code.:
DSSTox Substance ID:DTXSID90579396

Synonyms:87975-12-0;Phenyl 1-bromo-2-(cyclohexylamino)ethane-1-sulfonate;DTXSID90579396

Suppliers and Price of Phenyl 1-bromo-2-(cyclohexylamino)ethane-1-sulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenyl 1-bromo-2-(cyclohexylamino)ethane-1-sulfonate

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:361.03473
Heavy Atom Count:20
Complexity:370

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)NCC(S(=O)(=O)OC2=CC=CC=C2)Br

Technology Process of Phenyl 1-bromo-2-(cyclohexylamino)ethane-1-sulfonate

There total 4 articles about Phenyl 1-bromo-2-(cyclohexylamino)ethane-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 6904-89-8
Phenyl 1-bromoethenesulfonate

: 108-91-8,157973-60-9
cyclohexylamine

: 87975-12-0
1-Bromo-2-cyclohexylamino-ethanesulfonic acid phenyl ester

Guidance literature:: In benzene; for 24h; Ambient temperature;
DOI:10.1055/s-1983-30527

Reference yield: 60.0%

: 6855-00-1
Phenyl 1,2-dibromoethanesulfonate

: 108-91-8,157973-60-9
cyclohexylamine

: 87975-12-0
1-Bromo-2-cyclohexylamino-ethanesulfonic acid phenyl ester

Guidance literature:: In benzene; for 24h; Ambient temperature;
DOI:10.1055/s-1983-30527

Reference yield:

: 1562-34-1
phenyl vinylsulfonate

: 87975-12-0
1-Bromo-2-cyclohexylamino-ethanesulfonic acid phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Br₂, azodiisobutyronitrile / CCl₄ / 1.) reflux, 4 h; 2,) room temp., 48 h

2: 80 percent / triethylamine / benzene / 24 h / Ambient temperature

3: 60 percent / benzene / 24 h / Ambient temperature

With 2,2'-azobis(isobutyronitrile); bromine; triethylamine; In tetrachloromethane; benzene;
DOI:10.1055/s-1983-30527