Phosphoric acid, 1-cyano-1-phenylethyl diethyl ester

Base Information

Chemical Name:Phosphoric acid, 1-cyano-1-phenylethyl diethyl ester
CAS No.:88151-72-8
Molecular Formula:C13H18NO4P
Molecular Weight:283.264
Hs Code.:
DSSTox Substance ID:DTXSID40455171
Nikkaji Number:J3.243.885G

Synonyms:Phosphoric acid, 1-cyano-1-phenylethyl diethyl ester;88151-72-8;DTXSID40455171;Phosphoric acid alpha-cyano-alpha-methylbenzyl=diethyl ester

Suppliers and Price of Phosphoric acid, 1-cyano-1-phenylethyl diethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphoric acid, 1-cyano-1-phenylethyl diethyl ester

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:7
Exact Mass:283.09734505
Heavy Atom Count:19
Complexity:362

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOP(=O)(OCC)OC(C)(C#N)C1=CC=CC=C1

Technology Process of Phosphoric acid, 1-cyano-1-phenylethyl diethyl ester

There total 5 articles about Phosphoric acid, 1-cyano-1-phenylethyl diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 2942-58-7
diethyl cyanophosphonate

: 98-86-2
acetophenone

: 88151-72-8
1-(Diethylphosphonooxy)-2-phenylpropanenitrile

Guidance literature:: lithium diisopropyl amide; In tetrahydrofuran; at -10 - 22 ℃; for 1.83333h;

Reference yield: 87.0%

: 20435-05-6
phosphoric acid (phenyl)(cyano)methyl ester diethyl ester

: 74-88-4
methyl iodide

: 88151-72-8
1-(Diethylphosphonooxy)-2-phenylpropanenitrile

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; for 0.5h;

Reference yield:

: 100-52-7
benzaldehyde

: 88151-72-8
1-(Diethylphosphonooxy)-2-phenylpropanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / LiCN / tetrahydrofuran / Ambient temperature

2: 87 percent / n-BuLi, TMEDA / tetrahydrofuran; hexane / 0.5 h

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; lithium cyanide; In tetrahydrofuran; hexane;