1-Chloro-2-(dichloromethylidene)cyclohexane

Base Information

• Chemical Name: 1-Chloro-2-(dichloromethylidene)cyclohexane
• CAS No.: 88348-80-5
• Molecular Formula: C₇H₉Cl₃
• Molecular Weight: 199.507
• DSSTox Substance ID: DTXSID50574963
• Mol file: 88348-80-5.mol

Synonyms:1-Chloro-2-(dichloromethylidene)cyclohexane;88348-80-5;DTXSID50574963

Chemical Property of 1-Chloro-2-(dichloromethylidene)cyclohexane

Chemical Property:

• XLogP3: 3.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 197.976983
• Heavy Atom Count: 10
• Complexity: 147

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(=C(Cl)Cl)C(C1)Cl

Technology Process of 1-Chloro-2-(dichloromethylidene)cyclohexane

There total 2 articles about 1-Chloro-2-(dichloromethylidene)cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(trichloromethyl)cyclohexan-1-ol (3508-84-7) → 1-chloro-2-dichloromethylidenecyclohexane (88348-80-5)

Guidance literature:

With thionyl chloride;

DOI:10.1021/ja01604a041

Reference yield:

tetrachloromethane (56-23-5) + cyclohexene (110-83-8) → 1-chloro-2-trichloromethylcyclohexane (7484-12-0) + 1-trichloromethylcyclohexene (13875-80-4) + 1-chloro-2-dichloromethylidenecyclohexane (88348-80-5)

Guidance literature:

With copper tetra(tert-butyl)phthalocyanine; In acetonitrile; at 140 ℃; for 8h; Sealed tube;

DOI:10.1007/s11172-008-0377-0

upstream raw materials:

1-(trichloromethyl)cyclohexan-1-ol

tetrachloromethane

cyclohexene