N-[3-(Dimethylamino)-4-nitrophenyl]methanesulfonamide

Base Information

Chemical Name:N-[3-(Dimethylamino)-4-nitrophenyl]methanesulfonamide
CAS No.:88413-20-1
Molecular Formula:C9H13N3O4S
Molecular Weight:259.286
Hs Code.:
DSSTox Substance ID:DTXSID90548461
Wikidata:Q82427173

Synonyms:88413-20-1;N-[3-(Dimethylamino)-4-nitrophenyl]methanesulfonamide;DTXSID90548461

Suppliers and Price of N-[3-(Dimethylamino)-4-nitrophenyl]methanesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-[3-(Dimethylamino)-4-nitrophenyl]methanesulfonamide

Chemical Property:

XLogP3:0.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:259.06267708
Heavy Atom Count:17
Complexity:371

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C1=C(C=CC(=C1)NS(=O)(=O)C)[N+](=O)[O-]

Technology Process of N-[3-(Dimethylamino)-4-nitrophenyl]methanesulfonamide

There total 5 articles about N-[3-(Dimethylamino)-4-nitrophenyl]methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 124-63-0
methanesulfonyl chloride

: 55851-38-2
N,N-Dimethyl-2-Nitro-5-Aminoaniline

: 88413-20-1
3'-(dimethylamino)-4'-nitromethanesulfonanilide

Guidance literature:: With pyridine; at 20 ℃; for 4h;
DOI:10.1021/jm00387a012

Reference yield:

: 825-41-2
3-chloro-4-nitroaniline

: 88413-20-1
3'-(dimethylamino)-4'-nitromethanesulfonanilide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / pyridine / 1,2-dimethoxy-ethane / 1.) 20 deg C, 1 h, 2.) 100 deg C, 30 min

2: H₂O / 12 h / 100 °C

With pyridine; In 1,2-dimethoxyethane; water;
DOI:10.1021/jm00369a022

Reference yield:

: 712-33-4
3-chloro-4-nitroacetanilide

: 88413-20-1
3'-(dimethylamino)-4'-nitromethanesulfonanilide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂O / 3 h / 80 °C

2: 4N aq. HCl / ethanol / 3 h / Heating

3: 96 percent / pyridine / 4 h / 20 °C

With pyridine; hydrogenchloride; In ethanol; water;
DOI:10.1021/jm00387a012