1-Chloro-2-(2,2-dichloro-1-phenylethyl)benzene

Base Information

• Chemical Name: 1-Chloro-2-(2,2-dichloro-1-phenylethyl)benzene
• CAS No.: 61693-87-6
• Molecular Formula: C14H11Cl3
• Molecular Weight: 285.6
• NSC Number: 69821
• DSSTox Substance ID: DTXSID50290590
• Nikkaji Number: J2.359.461G

Synonyms:61693-87-6;1-chloro-2-(2,2-dichloro-1-phenylethyl)benzene;NSC69821;DTXSID50290590;NSC-69821

Chemical Property of 1-Chloro-2-(2,2-dichloro-1-phenylethyl)benzene

Chemical Property:

• Vapor Pressure: 2.87E-05mmHg at 25°C
• Boiling Point: 367.5°Cat760mmHg
• Flash Point: 255.9°C
• Density: 1.291g/cm³
• XLogP3: 5.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 283.992633
• Heavy Atom Count: 17
• Complexity: 224

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(C2=CC=CC=C2Cl)C(Cl)Cl

Technology Process of 1-Chloro-2-(2,2-dichloro-1-phenylethyl)benzene

There total 3 articles about 1-Chloro-2-(2,2-dichloro-1-phenylethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

methanol (67-56-1) + o,p'-DDT (789-02-6,58633-26-4) → 1,1'-ethylidenebis-benzene (612-00-0) + 1-Chloro-2-(2,2-dichloro-1-phenyl-ethyl)-benzene (61693-87-6) + 1,1-dichloro-2,2-diphenylethane (2387-16-8) + methyl 2,2-diphenylacetate (3469-00-9)

Guidance literature:

With hydrogen; triethylamine; palladium on activated charcoal; at 20 ℃; for 2h; Further byproducts given;

DOI:10.1016/j.tet.2006.06.041

Reference yield:

benzaldehyde (100-52-7) → 1-Chloro-2-(2,2-dichloro-1-phenyl-ethyl)-benzene (61693-87-6)

Guidance literature:

Multi-step reaction with 2 steps

1: nBuLi

2: SO₃/H₂SO₄

With n-butyllithium; sulfuric acid; sulfur trioxide;

Reference yield:

2,2-dichloro-1-phenylethanol (2612-36-4) + chlorobenzene (108-90-7) → 1-Chloro-2-(2,2-dichloro-1-phenyl-ethyl)-benzene (61693-87-6)

Guidance literature:

With sulfuric acid; sulfur trioxide;

upstream raw materials:

2,2-dichloro-1-phenylethanol

chlorobenzene

methanol

o,p'-DDT

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