Benzenesulfonamide, N-[1,2,3,3a,4,8b-hexahydro-3a-hydroxy-6,8b-dimethyl-1-oxo-4-(phenyl methyl)cyclopent[b]indol-7-yl]-4-methyl-N-(phenylmethyl)-

Base Information

• Chemical Name: Benzenesulfonamide, N-[1,2,3,3a,4,8b-hexahydro-3a-hydroxy-6,8b-dimethyl-1-oxo-4-(phenyl methyl)cyclopent[b]indol-7-yl]-4-methyl-N-(phenylmethyl)-
• CAS No.: 88589-37-1
• Molecular Formula: C₃₄H₃₄N₂O₄S
• Molecular Weight: 566.721

Synonyms:

Chemical Property of Benzenesulfonamide, N-[1,2,3,3a,4,8b-hexahydro-3a-hydroxy-6,8b-dimethyl-1-oxo-4-(phenyl methyl)cyclopent[b]indol-7-yl]-4-methyl-N-(phenylmethyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenesulfonamide, N-[1,2,3,3a,4,8b-hexahydro-3a-hydroxy-6,8b-dimethyl-1-oxo-4-(phenyl methyl)cyclopent[b]indol-7-yl]-4-methyl-N-(phenylmethyl)-

There total 6 articles about Benzenesulfonamide, N-[1,2,3,3a,4,8b-hexahydro-3a-hydroxy-6,8b-dimethyl-1-oxo-4-(phenyl methyl)cyclopent[b]indol-7-yl]-4-methyl-N-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

2,5-Bis-4-(2,5-dioxo-1-methylcyclopentyl)toluene (88589-36-0) → 4-Benzyl-7--6,8b-dimethyl-3a-hydroxy-1-oxo-1,2,3,3a,4,8b-hexahydrocyclopentindole (88589-37-1) + 1-Benzyl-8--6,9-dimethyl-2,5-dioxo-1,2,3,4,5,6-hexahydro-1-benzazocine (88589-39-3) + 1-Benzyl-8-(benzylamino)-6,9-dimethyl-2,5-dioxo-1,2,3,4,5,6-hexahydro-1-benzazocine (88609-66-9)

Guidance literature:

With anthracene; N,N,N,N-tetraethylammonium tetrafluoroborate; In N,N-dimethyl-formamide; for 0.133333h; electrolysis with Hg cathode at -2.00 V vs. Pt, carbon rod as anode;

DOI:10.1021/jo00180a001

Reference yield: 14.0%

methanol (67-56-1) + 2,5-Bis-4-(2,5-dioxo-1-methylcyclopentyl)toluene (88589-36-0) → 4-Benzyl-7--6,8b-dimethyl-3a-hydroxy-1-oxo-1,2,3,3a,4,8b-hexahydrocyclopentindole (88589-37-1) + 2,5-Bis-4-(1-methyl-2-oxo-4-carbomethoxybutyl)toluene (88589-40-6)

Guidance literature:

With N,N,N,N-tetraethylammonium tetrafluoroborate; In N,N-dimethyl-formamide; for 1h; electrolysis with Pb plate as cathode at -1.7 V vs. Pt;

DOI:10.1021/jo00180a001

Reference yield: 5.0%

ethanol (64-17-5) + 2,5-Bis-4-(2,5-dioxo-1-methylcyclopentyl)toluene (88589-36-0) → 4-Benzyl-7--6,8b-dimethyl-3a-hydroxy-1-oxo-1,2,3,3a,4,8b-hexahydrocyclopentindole (88589-37-1) + 2,5-Bis-4-(1-methyl-2-oxo-4-carboethoxybutyl)toluene (88589-41-7)

Guidance literature:

With tetraethylammonium tosylate; In N,N-dimethyl-formamide; for 0.116667h; electrolysis with Pb cathode at -1.7 V vs. Pt;

DOI:10.1021/jo00180a001

upstream raw materials:

methanol

2,5-Bis-4-(2,5-dioxo-1-methylcyclopentyl)toluene

ethanol

C₂₇H₂₈N₂O₆S₂

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