PAA-HCL 10L

Base Information

• Chemical Name: PAA-HCL 10L
• CAS No.: 110507-15-8
• Molecular Formula: C₃H₈N*Cl
• Molecular Weight: 93.5562
• Mol file: 110507-15-8.mol

Synonyms:

Chemical Property of PAA-HCL 10L

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of PAA-HCL 10L

There total 10 articles about PAA-HCL 10L which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N,N-bis(trimethylsilyl)allylamine (7688-51-9) → Hexamethyldisiloxane (107-46-0) + allylammonium chloride (10017-11-5,110507-15-8,71550-12-4)

Guidance literature:

With hydrogenchloride; In diethyl ether;

Reference yield: 99.0%

N-tert-butoxycarbonylprop-2-en-1-amine (78888-18-3) → allylammonium chloride (10017-11-5,110507-15-8,71550-12-4)

Guidance literature:

With sulfuric acid; sodium chloride; In neat (no solvent); at 20 ℃; for 1h; Sealed tube;

DOI:10.1039/d1ob00728a

Reference yield: 67.0%

C12H24NO5P (85231-93-2) → allylammonium chloride (10017-11-5,110507-15-8,71550-12-4)

Guidance literature:

With hydrogenchloride; In benzene; Ambient temperature;

DOI:10.1055/s-1982-29997

upstream raw materials:

N,N-bis(trimethylsilyl)allylamine

C₁₂H₂₄NO₅P

N-tritylprop-2-en-1-amine

1-bromo dodecane

Downstream raw materials:

(S,R)-3-bromo-5-aminomethyl-4,5-dihydroisoxazole

(R)-(3-bromo-4,5-dihydroisoxazol-5-yl)methanamine

(S)-(3-bromo-4,5-dihydroisoxazol-5-yl)methanamine

N-allylphenethylamine

Refernces

• 1、 Bhunia, Mrinal,Sahoo, Sumeet Ranjan,Das, Arpan,Ahmed, Jasimuddin,Sreejyothi,Mandal, Swadhin K.. "Transition metal-free catalytic reduction of primary amides using an abnormal NHC based potassium complex: Integrating nucleophilicity with Lewis acidic activation". . p. 1848 - 1854. Retrieved 2020/03/03.
• 2、 Theodorou, Vassiliki,Ragoussis, Valentine,Strongilos, Alexandros,Zelepos, Evangelos,Eleftheriou, Argyro,Dimitriou, Maria. "A convenient method for the preparation of primary amines using tritylamine". . p. 1357 - 1360. Retrieved 2007/10/03.