4-Amino-4'-(dimethylamino)benzophenone

Base Information

• Chemical Name: 4-Amino-4'-(dimethylamino)benzophenone
• CAS No.: 5809-25-6
• Molecular Formula: C15H16N2O
• Molecular Weight: 240.305
• European Community (EC) Number: 611-620-1
• DSSTox Substance ID: DTXSID60206809
• Wikidata: Q83080660
• Mol file: 5809-25-6.mol

Synonyms:4-Amino-4'-(dimethylamino)benzophenone;5809-25-6;Benzophenone, 4-amino-4'-(dimethylamino)-;SCHEMBL6113062;DTXSID60206809;SY310615;(4-Aminophenyl)[4-(dimethylamino)phenyl]methanone;4-aminophenyl[4'-(dimethylamino)phenyl]-methanone;(4-Amino-phenyl)-(4-dimethylamino-phenyl)-methanone

Chemical Property of 4-Amino-4'-(dimethylamino)benzophenone

Chemical Property:

• Vapor Pressure: 6.88E-08mmHg at 25°C
• Boiling Point: 438.5°Cat760mmHg
• Flash Point: 219°C
• Density: 1.156g/cm³
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 240.126263138
• Heavy Atom Count: 18
• Complexity: 274

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=CC=C(C=C1)C(=O)C2=CC=C(C=C2)N

Technology Process of 4-Amino-4'-(dimethylamino)benzophenone

There total 5 articles about 4-Amino-4'-(dimethylamino)benzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

tert-butyl 4-[4'-(dimethylamino)benzoyl] phenylcarbamate (1217306-78-9) → 4-aminophenyl-[4'-(dimethylamino)phenyl] methanone (5809-25-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1039/b921550f

Reference yield:

crystal violet (548-62-9) → N,N',N''-trimethylpararosaniline + N,N'-dimethylpararosaniline + N-methyl-p-aminophenol (150-75-4) + 4-(N-methylamino)-4'-aminobenzophenone (81260-56-2) + 4-(N,N-dimethylamino)phenol (619-60-3) + 4,4'-diaminobenzophenone (611-98-3) + 4-(N-methylamino)-4'-(N'-methylamino)benzophenone (3708-39-2) + C22H24N3(1+)*Cl(1-) + C21H22N3(1+)*Cl(1-) + C20H20N3(1+)*Cl(1-) + C23H26N3(1+)*Cl(1-) + (4-(dimethylamino)phenyl)(4-(methylamino)phenyl)methanone (81260-55-1) + 4-amino-phenol (123-30-8) + methyl violet 2B (71143-08-3) + basic red 9 (569-61-9,131883-55-1,187112-40-9) + crystal violet chloride + bis(p-dimethylaminophenyl)methanone (90-94-8) + 4-aminophenyl-[4'-(dimethylamino)phenyl] methanone (5809-25-6)

Guidance literature:

With bismuth oxyiodide grafted graphene oxide nanosheet; pH=7; Reagent/catalyst; pH-value; Kinetics; UV-irradiation;

DOI:10.1039/c6ra12482h

Reference yield:

Malachitgruen (569-64-2,38676-32-3) → 4-(Dimethylamino)benzophenone (530-44-9) + (4-(methylamino)phenyl)(phenyl)methanone (26178-74-5) + 2-hydroxyl-4-dimethylaminobenzophenone + 4-aminophenyl-[4'-(dimethylamino)phenyl] methanone (5809-25-6)

Guidance literature:

With dihydrogen peroxide; iron(III) perchlorate; p-benzoquinone; In water; for 0.333333h; Further Variations:; Reagents; Catalysts; without visible light irradiation; reaction time; Product distribution; Irradiation;

DOI:10.1039/b107404k

upstream raw materials:

Malachitgruen

(4-(dimethylamino)phenyl)(4-nitrophenyl)methanone

tert-butyl 4-[4'-(dimethylamino)benzoyl] phenylcarbamate

bis(p-dimethylaminophenyl)methanone

Refernces

• 1、 -. "SURFACE ENHANCED RAMAN SPECTROSCOPY (SERS) COMPOUNDS AND METHODS OF THEIR PREPARATION". . . Retrieved 2012/06/01.
• 2、 Lu, Chung-Shin,Mai, Fu-Der,Wu, Yi-Chin,Yao, I-Chun,Hsu, Peng-Yueh,Chen, Chiing-Chang. "Photocatalytic degradation of michler's ketone in water by Uv light illumination using TiO2 photocatalyst: Identification of intermediates and the reaction pathway". experimental part. p. 729 - 740. Retrieved 2010/08/19.