Diazenecarboxylic acid, phenyl-, ethyl ester

Base Information

Chemical Name:Diazenecarboxylic acid, phenyl-, ethyl ester
CAS No.:943-76-0
Molecular Formula:C9H10N2O2
Molecular Weight:178.191
Hs Code.:
DSSTox Substance ID:DTXSID20439914
Nikkaji Number:J2.825.686H

Synonyms:943-76-0;Diazenecarboxylic acid, phenyl-, ethyl ester;SCHEMBL17182758;DTXSID20439914;3-Phenyl-2,3-didehydrocarbazic acid ethyl ester

Suppliers and Price of Diazenecarboxylic acid, phenyl-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Diazenecarboxylic acid, phenyl-, ethyl ester

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:178.074227566
Heavy Atom Count:13
Complexity:186

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)N=NC1=CC=CC=C1

Technology Process of Diazenecarboxylic acid, phenyl-, ethyl ester

There total 8 articles about Diazenecarboxylic acid, phenyl-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 6233-02-9
ethyl phenylhydrazocarboxylate

: 943-76-0
ethyl 2-phenyldiazenecarboxylate

Guidance literature:: With ammonium cerium (IV) nitrate; In methanol; at 20 ℃;
DOI:10.1016/j.tet.2010.02.042

Reference yield:

: 100-63-0
phenylhydrazine

: 943-76-0
ethyl 2-phenyldiazenecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

2: potassium permanganate; water; glacial acetic acid

With potassium permanganate; water; acetic acid;

Reference yield:

: 100-63-0
phenylhydrazine

: 943-76-0
ethyl 2-phenyldiazenecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / pyridine / 0 - 25 °C

2: 91 percent / Pb(OAc)4 / CH₂Cl₂ / 0.5 h / 0 °C

With lead(IV) acetate; In pyridine; dichloromethane;
DOI:10.1021/jo990750v