Benzyl 6-oxohexylcarbamate

Base Information

Chemical Name:Benzyl 6-oxohexylcarbamate
CAS No.:98648-05-6
Molecular Formula:C14H19NO3
Molecular Weight:249.31
Hs Code.:
European Community (EC) Number:894-437-1
Nikkaji Number:J2.561.721E

Synonyms:Benzyl 6-oxohexylcarbamate;98648-05-6;Benzyl (6-oxohexyl)carbamate;Benzyl N-(6-oxohexyl)carbamate;Benzyl(6-oxohexyl)carbamate;benzyl-(6-oxohexyl)carbamate;LCZC2147;SCHEMBL6444628;XPGMGPSEWHRDSL-UHFFFAOYSA-N;6-(N-benzyloxycarbonylamino)hexanal;YDA64805;MFCD12031811;AKOS027338588;AS-30332;BP-28383;A1-17775

Suppliers and Price of Benzyl 6-oxohexylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Benzyl 6-oxohexylcarbamate

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:9
Exact Mass:249.13649347
Heavy Atom Count:18
Complexity:237

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC(=O)NCCCCCC=O

Technology Process of Benzyl 6-oxohexylcarbamate

There total 8 articles about Benzyl 6-oxohexylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 17996-12-2
N-benzyloxycarbonyl-6-amino-1-hexanol

: 98648-05-6
6-oxo-hexyl-carbamic acid benzyl ester

Guidance literature:: With pyridinium chlorochromate; In tetrahydrofuran; at 0 ℃;
DOI:10.1002/pola.28468

Reference yield:

N-hydrochloric acid: N-hydrochloric acid

: 79-37-8
oxalyl dichloride

: 17996-12-2
N-benzyloxycarbonyl-6-amino-1-hexanol

: 7087-68-5
N-ethyl-N,N-diisopropylamine

: 98648-05-6
6-oxo-hexyl-carbamic acid benzyl ester

Guidance literature:: With dimethyl sulfoxide; In ice-water; dichloromethane; ethyl acetate;

Reference yield:

: 4048-33-3
6-amino-1-hexanol

: 98648-05-6
6-oxo-hexyl-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / acetone / 24 h / 20 °C

2: magnesium sulfate; pyridinium chlorochromate / dichloromethane / 4 h / 20 °C

With sodium hydrogencarbonate; magnesium sulfate; pyridinium chlorochromate; In dichloromethane; acetone;
DOI:10.1002/asia.201000873