3-Bromo-N-(4-fluorobenzoyl)benzene-1-carbohydrazonic acid

Base Information

Chemical Name:3-Bromo-N-(4-fluorobenzoyl)benzene-1-carbohydrazonic acid
CAS No.:5279-82-3
Molecular Formula:C₁₀H₉N
Molecular Weight:143.188
Hs Code.:
DSSTox Substance ID:DTXSID10967251
Wikidata:Q82949832
Mol file:5279-82-3.mol

Synonyms:5279-82-3;3-Bromo-N-(4-fluorobenzoyl)benzene-1-carbohydrazonic acid;DTXSID10967251;AKOS017053027;SR-01000203125;SR-01000203125-1

Suppliers and Price of 3-Bromo-N-(4-fluorobenzoyl)benzene-1-carbohydrazonic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-Bromo-N-(4-fluorobenzoyl)benzene-1-carbohydrazonic acid

Chemical Property:

Boiling Point:550.8°Cat760mmHg
Flash Point:286.9°C
Density:1.543g/cm³
XLogP3:3.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:335.99097
Heavy Atom Count:20
Complexity:359

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=CC(=C1)Br)C(=O)NNC(=O)C2=CC=C(C=C2)F

Technology Process of 3-Bromo-N-(4-fluorobenzoyl)benzene-1-carbohydrazonic acid

There total 17 articles about 3-Bromo-N-(4-fluorobenzoyl)benzene-1-carbohydrazonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 6011-14-9
2-aminoacetonitrile hydrochloride

: 4660-02-0,5279-82-3,5590-14-7,58626-34-9,58626-35-0,58641-88-6,58641-89-7,68907-36-8,68907-41-5
(+/-)-trans-2-phenylcyclopropanecarbonitrile

: 4660-02-0,5279-82-3,5590-14-7,58626-34-9,58626-35-0,58641-88-6,58641-89-7,68907-36-8,68907-41-5
cis-2-phenylcyclopropanecarbonitrile

Guidance literature:: With meso-tetraphenylporphyrin iron(III) chloride; sodium nitrite; In dichloromethane; water; at 20 ℃; for 14h; Solvent; Temperature; Reagent/catalyst; diastereoselective reaction; Inert atmosphere; Green chemistry;
DOI:10.1039/c7gc00602k

Reference yield: 81.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 6011-14-9
2-aminoacetonitrile hydrochloride

: 4660-02-0,5279-82-3,5590-14-7,58626-34-9,58626-35-0,58641-88-6,58641-89-7,68907-36-8,68907-41-5
(+/-)-trans-2-phenylcyclopropanecarbonitrile

: 4660-02-0,5279-82-3,5590-14-7,58626-34-9,58626-35-0,58641-88-6,58641-89-7,68907-36-8,68907-41-5
cis-2-phenylcyclopropanecarbonitrile

Guidance literature:: With meso-tetraphenylporphyrin iron(III) chloride; sodium nitrite; In dichloromethane; water; at 20 ℃; for 14h; Solvent; Temperature; Reagent/catalyst; diastereoselective reaction; Inert atmosphere; Green chemistry;
DOI:10.1039/c7gc00602k

Reference yield: 5.0%

: 1885-38-7
cinnamic nitrile

: 1774-47-6
trimethylsulfoxonium iodide

: 4660-02-0,5279-82-3,5590-14-7,58626-34-9,58626-35-0,58641-88-6,58641-89-7,68907-36-8,68907-41-5
(+/-)-trans-2-phenylcyclopropanecarbonitrile

Guidance literature:: cinnamic nitrile; trimethylsulfoxonium iodide; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 19h; Inert atmosphere;

In N,N-dimethyl-formamide; at 50 ℃; for 8h; Inert atmosphere;
DOI:10.1021/acs.organomet.9b00290