1,7,7-Trimethyl-2-norbornanone dimethyl ketal

Base Information

Chemical Name:1,7,7-Trimethyl-2-norbornanone dimethyl ketal
CAS No.:10395-50-3
Molecular Formula:C₁₂H₂₂O₂
Molecular Weight:198.305
Hs Code.:
DSSTox Substance ID:DTXSID60908679
Nikkaji Number:J2.632.005D
Mol file:10395-50-3.mol

Synonyms:10395-50-3;1,7,7-Trimethyl-2-norbornanone dimethyl ketal;2,2-Dimethoxy-1,7,7-trimethyl-norbornane;128525-51-9;109280-15-1;camphor dimethyl acetal;SCHEMBL1823706;DTXSID60908679;2,2-DIMETHOXY-1,7,7-TRIMETHYLBICYCLO[2.2.1]HEPTANE

Suppliers and Price of 1,7,7-Trimethyl-2-norbornanone dimethyl ketal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1,7,7-Trimethyl-2-norbornanone dimethyl ketal

Chemical Property:

Vapor Pressure:0.236mmHg at 25°C
Boiling Point:213.7°Cat760mmHg
Flash Point:58.3°C
Density:0.97g/cm³
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:198.161979940
Heavy Atom Count:14
Complexity:243

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C2CCC1(C(C2)(OC)OC)C)C

Technology Process of 1,7,7-Trimethyl-2-norbornanone dimethyl ketal

There total 2 articles about 1,7,7-Trimethyl-2-norbornanone dimethyl ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 736109-58-3,787517-91-3,68546-28-1
1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one

: 149-73-5
trimethyl orthoformate

: 10395-50-3
2,2-dimethoxy-1,7,7-trimethylbicyclo<2.2.1>heptane

Guidance literature:: With toluene-4-sulfonic acid; In methanol; Heating;
DOI:10.1021/jo00289a051

Reference yield:

: 67-56-1
methanol

: 736109-58-3,787517-91-3,68546-28-1
1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one

: 10395-50-3
2,2-dimethoxy-1,7,7-trimethylbicyclo<2.2.1>heptane

Guidance literature:: With chloranil; In acetonitrile; for 0.5h; Irradiation;
DOI:10.1021/jo0485886

Reference yield:

: 10395-50-3
2,2-dimethoxy-1,7,7-trimethylbicyclo<2.2.1>heptane

: 131146-91-3,131233-71-1,135267-00-4,1214020-75-3
(+/-)-4-O-allyl-1,5,6-tri-O-benzyl-myo-inositol

: 1323371-30-7
6-O-allyl-3,4,5-tri-O-benzyl-1,2-O-{(+)-1,7,7-trimethyl[2,2,1]bicyclohepta-6-ylidene}-D-myo-inositol

: 6-O-allyl-3,4,5-tri-O-benzyl-1,2-O-{(+)-1,1,7-trimethyl[2,2,1]bicyclohepta-6-ylidene}-L-myo-inositol

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; for 2h; Overall yield = 43.6 %; Overall yield = 5 g; Inert atmosphere; Reflux;
DOI:10.1039/c3ob42116c