N-(2,2-diethoxyethyl)-1-(6-methoxy-1,4-dimethyl-9H-carbazol-3-yl)methanimine

Base Information

Chemical Name:N-(2,2-diethoxyethyl)-1-(6-methoxy-1,4-dimethyl-9H-carbazol-3-yl)methanimine
CAS No.:18073-24-0
Molecular Formula:C22H28N2O3
Molecular Weight:368.476
Hs Code.:
NSC Number:143117
DSSTox Substance ID:DTXSID50301397
Mol file:18073-24-0.mol

Synonyms:18073-24-0;N-(2,2-diethoxyethyl)-1-(6-methoxy-1,4-dimethyl-9H-carbazol-3-yl)methanimine;NSC143117;DTXSID50301397;NSC-143117

Suppliers and Price of N-(2,2-diethoxyethyl)-1-(6-methoxy-1,4-dimethyl-9H-carbazol-3-yl)methanimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of N-(2,2-diethoxyethyl)-1-(6-methoxy-1,4-dimethyl-9H-carbazol-3-yl)methanimine

Chemical Property:

Vapor Pressure:3.53E-11mmHg at 25°C
Boiling Point:539.9°Cat760mmHg
Flash Point:280.3°C
Density:1.13g/cm³
XLogP3:4.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:368.20999276
Heavy Atom Count:27
Complexity:480

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(CN=CC1=C(C2=C(C(=C1)C)NC3=C2C=C(C=C3)OC)C)OCC

Technology Process of N-(2,2-diethoxyethyl)-1-(6-methoxy-1,4-dimethyl-9H-carbazol-3-yl)methanimine

There total 5 articles about N-(2,2-diethoxyethyl)-1-(6-methoxy-1,4-dimethyl-9H-carbazol-3-yl)methanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 18073-15-9
6-methoxy-1,4-dimethyl-9-H-carbazole-3-carbaldehyde

: 645-36-3
2,2-diethoxy-ethanamine

: 18073-24-0
dimethyl-1,4 (diethoxy-2,2 ethyliminomethyl)-3 methoxy-6 carbazole

Guidance literature:

Reference yield:

: 18028-57-4
6-methoxy-1,4-dimethyl-9H-carbazole

: 18073-24-0
dimethyl-1,4 (diethoxy-2,2 ethyliminomethyl)-3 methoxy-6 carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / phosphorus oxychloride / trichloroethene / 4 h / 100 °C

2: 87 percent

With trichlorophosphate; In Trichloroethylene;

Reference yield:

: 1006-94-6
5-methoxylindole

: 18073-24-0
dimethyl-1,4 (diethoxy-2,2 ethyliminomethyl)-3 methoxy-6 carbazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: Montmorillonite powder preloaded with p-toluenesulfonic acid / 0.17 h / Microwave irradiation

2.1: trichlorophosphate / 0.5 h / Cooling with ice

2.2: 48 h / 20 °C / Cooling with ice; Inert atmosphere

3.1: 3 h / 130 °C

With trichlorophosphate;