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1-Phenyl-1,3-hexadiyne

Base Information Edit
  • Chemical Name:1-Phenyl-1,3-hexadiyne
  • CAS No.:10508-66-4
  • Molecular Formula:C12H10
  • Molecular Weight:0
  • Hs Code.:
  • Mol file:10508-66-4.mol
1-Phenyl-1,3-hexadiyne

Synonyms:1,3-Hexadiyne,1-phenyl- (7CI,8CI); Benzene, 1,3-hexadiynyl- (9CI); 1-Phenyl-1,3-hexadiyne;Neocapillen

Suppliers and Price of 1-Phenyl-1,3-hexadiyne
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
Total 3 raw suppliers
Chemical Property of 1-Phenyl-1,3-hexadiyne Edit
Chemical Property:
  • Boiling Point:85 - 90 °C (0.05 mmHg) 
  • PSA:0.00000 
  • LogP:2.45150 
Purity/Quality:

98%,99%, *data from raw suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
Technology Process of 1-Phenyl-1,3-hexadiyne

There total 9 articles about 1-Phenyl-1,3-hexadiyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
phenylacetylene; With hydroxylamine hydrochloride; N-butylamine; copper(l) chloride; In tetrahydrofuran; water; at 0 ℃; Inert atmosphere;
1-bromobut-1-yne; In tetrahydrofuran; water; at 0 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/acs.orglett.8b02975
Guidance literature:
(1,1-dibromobut-1-en-3-yn-2-yl)benzene; With n-butyllithium; In hexane; toluene; at -20 - 0 ℃;
ethyl iodide; In diethyl ether; hexane; toluene; at -20 - 20 ℃; Further stages.;
DOI:10.1055/s-2007-1000937
Guidance literature:
Multi-step reaction with 3 steps
1: 50 percent / PCl5
2: 63 percent / Et3N / petroleum ether / 18 h / Ambient temperature
3: 1.) 15 percent BuLi / 1.) ether, hexane, -70 to 10 deg C, 3 h, 2.) ether, hexane, HMPT, -60 to 15 deg C, 3 h
With n-butyllithium; phosphorus pentachloride; triethylamine; In Petroleum ether;
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