4,4'-Methylenedibenzonitrile

Base Information

Chemical Name:4,4'-Methylenedibenzonitrile
CAS No.:10466-37-2
Molecular Formula:C15H10N2
Molecular Weight:218.258
Hs Code.:2926909090
NSC Number:174860
UNII:03E7XYB5GF
DSSTox Substance ID:DTXSID20306278
Nikkaji Number:J836.542C
Wikidata:Q72468573
Mol file:10466-37-2.mol

Synonyms:10466-37-2;4,4'-Methylenedibenzonitrile;4,4'-Dicyanodiphenylmethane;4-[(4-cyanophenyl)methyl]benzonitrile;4,4'-(1-methylene) bis-Benzonitrile;4,4'-Methylenebisbenzonitrile;03E7XYB5GF;NSC-174860;4,4/'-(1-METHYLENE) BIS-BENZONITRILE;4-((4-cyanophenyl)methyl)benzonitrile;NSC174860;UNII-03E7XYB5GF;SCHEMBL1344068;DTXSID20306278;AMY38139;AC-608;4,4-(1-methylene) bis-Benzonitrile;AKOS015918401;NSC 174860;BS-52257;CS-0339655;FT-0652352;E77204;A801029;Benzonitrile, 4,4'-methylenebis-;Benzonitrile, 4,4'-methylenedi- (6CI,7CI,8CI);4,4'-Methylenebis[benzonitrile]

Suppliers and Price of 4,4'-Methylenedibenzonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4,4''-(1-Methylene)bis-Benzonitrile
100mg
$ 260.00

TRC
4,4''-(1-Methylene)bis-Benzonitrile
10mg
$ 45.00

American Custom Chemicals Corporation
4,4'-(1-METHYLENE) BIS-BENZONITRILE 95.00%
5G
$ 3811.50

Total 42 raw suppliers

Chemical Property of 4,4'-Methylenedibenzonitrile

Chemical Property:

Appearance/Colour:White solid
Melting Point:167 °C
Boiling Point:410.6 °C at 760 mmHg
Flash Point:199.6 °C
PSA：47.58000
Density:1.17 g/cm³
LogP:3.02076
Storage Temp.:Room Temperature, under inert atmosphere
Solubility.:Chloroform (Slightly)
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:218.084398327
Heavy Atom Count:17
Complexity:292

Purity/Quality:

99% ^*data from raw suppliers

4,4''-(1-Methylene)bis-Benzonitrile ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1CC2=CC=C(C=C2)C#N)C#N

Technology Process of 4,4'-Methylenedibenzonitrile

There total 17 articles about 4,4'-Methylenedibenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 623-03-0
4-Cyanochlorobenzene

: 104-85-8
para-methylbenzonitrile

: 10466-37-2
4,4'-dicyanodiphenylmethane

Guidance literature:: para-methylbenzonitrile; With n-butyllithium; In tetrahydrofuran; at -60 ℃; for 0.5h;

4-Cyanochlorobenzene; In tetrahydrofuran; at -60 - -50 ℃; for 2h; Reagent/catalyst; Temperature;

Reference yield: 60.0%

: 75-09-2
dichloromethane

: 623-00-7
4-bromobenzenecarbonitrile

: 10466-37-2
4,4'-dicyanodiphenylmethane

Guidance literature:: dichloromethane; With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; triethylamine; 4,4'-di-tert-butyl-2,2'-bipyridine; at 20 ℃; for 0.5h; Inert atmosphere; Schlenk technique; Sealed tube;

4-bromobenzenecarbonitrile; at 20 ℃; for 20h; Irradiation; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1021/acs.orglett.0c03248

Reference yield: 55.0%

: 112809-51-5
letrozol

: 10466-37-2
4,4'-dicyanodiphenylmethane

Guidance literature:: With tetraethylammonium perchlorate; triethylamine; In dimethyl sulfoxide; at 20 ℃; for 6h; Electrolysis; Green chemistry;
DOI:10.1039/d1gc00317h