n,n-Dibutylpent-2-yn-1-amine

Base Information

• Chemical Name: n,n-Dibutylpent-2-yn-1-amine
• CAS No.: 6323-75-7
• Molecular Formula: C13H25N
• Molecular Weight: 195.348
• NSC Number: 34147
• DSSTox Substance ID: DTXSID10283908
• Nikkaji Number: J3.323.734K
• Wikidata: Q82018655
• Mol file: 6323-75-7.mol

Synonyms:6323-75-7;n,n-dibutylpent-2-yn-1-amine;NSC34147;DTXSID10283908;NSC-34147

Chemical Property of n,n-Dibutylpent-2-yn-1-amine

Chemical Property:

• Vapor Pressure: 0.0131mmHg at 25°C
• Boiling Point: 259.3°Cat760mmHg
• Flash Point: 101.1°C
• Density: 0.835g/cm³
• XLogP3: 3.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 7
• Exact Mass: 195.198699802
• Heavy Atom Count: 14
• Complexity: 164

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCN(CCCC)CC#CCC

Technology Process of n,n-Dibutylpent-2-yn-1-amine

There total 1 articles about n,n-Dibutylpent-2-yn-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl bromide (74-96-4) + 3-(dibutylamino)-1-propyne (6336-58-9) → N,N-dibutylpent-2-yn-1-amine (6323-75-7)

Guidance literature:

With ammonia; sodium amide;

DOI:10.1021/ja01163a600

Reference yield: 33.0%

N,N-dibutylpent-2-yn-1-amine (6323-75-7) + Phenyl azide (622-37-7) → 1-(1-phenyl-1H-1,2,3-triazol-4-yl)propan-1-one (1571095-49-2)

Guidance literature:

N,N-dibutylpent-2-yn-1-amine; With peroxyacetic acid; In ethanol; at 85 ℃; for 1h;

Phenyl azide; With sodium carbonate; In ethanol; at 85 ℃; for 18h;

DOI:10.1021/ol501842b

Reference yield:

N,N-dibutylpent-2-yn-1-amine (6323-75-7) → 1-dibutylamino-4-pentyne (74612-43-4) + dibutylamide of valeric acid (14313-88-3) + 1-dibutylamino-3-pentyne (79543-68-3) + dibutylamine (111-92-2)

Guidance literature:

With lithium 2-aminoethylamide; In ethylenediamine; at 0 ℃; for 1h; Product distribution; var. solvents, var. ratio of reagent : input compound;

upstream raw materials:

ethyl bromide

3-(dibutylamino)-1-propyne

Downstream raw materials:

1-dibutylamino-4-pentyne

dibutylamide of valeric acid

1-dibutylamino-3-pentyne

dibutylamine