n'-Benzoyl-4-chlorobenzohydrazide

Base Information

• Chemical Name: n'-Benzoyl-4-chlorobenzohydrazide
• CAS No.: 6828-55-3
• Molecular Formula: C14H11ClN2O2
• Molecular Weight: 274.707
• European Community (EC) Number: 654-569-0
• NSC Number: 83243
• DSSTox Substance ID: DTXSID90987811
• Nikkaji Number: J3.043.927I
• Wikidata: Q82976148
• Mol file: 6828-55-3.mol

Synonyms:n'-benzoyl-4-chlorobenzohydrazide;NSC83243;SCHEMBL4619519;DTXSID90987811;NSC-83243;AKOS003410240;N-(4-Chlorobenzoyl)benzenecarbohydrazonato;I+/--Benzoyl-I(2)-p-chlorbenzoyl-hydrazid;1-BENZOYL-2-(4-CHLOROBENZOYL)HYDRAZINE

Chemical Property of n'-Benzoyl-4-chlorobenzohydrazide

Chemical Property:

• Boiling Point: 524°Cat760mmHg
• Flash Point: 270.7°C
• Density: 1.308g/cm³
• XLogP3: 2.4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 274.0509053
• Heavy Atom Count: 19
• Complexity: 321

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=O)NNC(=O)C2=CC=C(C=C2)Cl

Technology Process of n'-Benzoyl-4-chlorobenzohydrazide

There total 7 articles about n'-Benzoyl-4-chlorobenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

benzoic acid hydrazide (613-94-5) + 4-chlorobenzoic acid hydrazide (536-40-3) → N'-benzoylbenzohydrazide (787-84-8) + N'-benzoyl-4′-chlorobenzohydrazide (6828-55-3) + N,N'-bis(p-chlorobenzoyl)hydrazine (895-84-1)

Guidance literature:

With [bis(acetoxy)iodo]benzene; In acetonitrile; for 0.0833333h; Heating;

DOI:10.1080/00397919708005637

Reference yield:

benzoyl chloride (98-88-4) + 4-chlorobenzoic acid hydrazide (536-40-3) → N'-benzoyl-4′-chlorobenzohydrazide (6828-55-3)

Guidance literature:

With pyridine; Heating;

DOI:10.1002/mrc.2804

Reference yield:

2-benzoyl-4,5-dichloropyridazin-3(2H)-one (155164-66-2) + 4,5-dichloro-2-(4-chloro-benzoyl)-2H-pyridazin-3-one (450408-66-9) → N'-benzoyl-4′-chlorobenzohydrazide (6828-55-3)

Guidance literature:

2-benzoyl-4,5-dichloropyridazin-3(2H)-one; With hydrazine hydrate; In tetrahydrofuran; at 20 ℃; for 0.166667h;

4,5-dichloro-2-(4-chloro-benzoyl)-2H-pyridazin-3-one; In tetrahydrofuran; at 20 ℃; for 0.166667h;

DOI:10.1055/s-2003-37647

upstream raw materials:

benzoic acid hydrazide

4-chlorobenzoic acid hydrazide

2-benzoyl-4,5-dichloropyridazin-3(2H)-one

4,5-dichloro-2-(4-chloro-benzoyl)-2H-pyridazin-3-one

Downstream raw materials:

4-Chlor-azodibenzoyl

2-(4-chlorophenyl)-5-phenyl-1,3,4-selenadiazole

3-(4-chlorophenyl)-4-methyl-5-phenyl-4H-1,2,4-triazole

3-(4-chlorophenyl)-5-phenyl-1H-1,2,4-triazole