N-(Trimethylsilyl)-N-[2-(trimethylsiloxy)ethyl]trimethylsilanamine

Base Information

• Chemical Name: N-(Trimethylsilyl)-N-[2-(trimethylsiloxy)ethyl]trimethylsilanamine
• CAS No.: 5630-81-9
• Molecular Formula: C17H12ClN5O5
• Molecular Weight: 277.63
• Mol file: 5630-81-9.mol

Synonyms:N,N,O-tris(trimethylsilyl) 2-aminoethanol;Trimethyl-[2-(bis-trimethylsilylamino)-ethoxy]-silan;N,N,O-Tris(trimethylsilyl)-2-aminoethanol;O,N,N-Tri-(trimethylsilyl)-β-aminoaethanol;[2-(Bis-trimethylsilyl-amino)-ethoxy]-trimethyl-silan;Tris-trimethylsilyl-ethanolamin;

Chemical Property of N-(Trimethylsilyl)-N-[2-(trimethylsiloxy)ethyl]trimethylsilanamine

Chemical Property:

• Vapor Pressure: 3.93E-11mmHg at 25°C
• Boiling Point: 525.4°C at 760 mmHg
• PKA: 14.00±0.70(Predicted)
• Flash Point: 271.6°C
• PSA: 12.47000
• Density: 1.56g/cm³
• LogP: 3.80970

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(Trimethylsilyl)-N-[2-(trimethylsiloxy)ethyl]trimethylsilanamine

There total 2 articles about N-(Trimethylsilyl)-N-[2-(trimethylsiloxy)ethyl]trimethylsilanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.4%

trimethylsilyl trifluoromethanesulfonate (27607-77-8) + 2-(trimethylsiloxy)-N-(trimethylsilyl)ethylamine (17165-52-5) → N-(2-trimethylsiloxyethyl)hexamethyldisilazane (5630-81-9)

Guidance literature:

With triethylamine; at 80 ℃; for 6h;

Reference yield:

→ N-(2-trimethylsiloxyethyl)hexamethyldisilazane (5630-81-9)

Guidance literature:

Ethanolamin, 1. Trimethylsilyl-diethylamin, Spatelspitze Ammoniumsulfat bis alles Diethylamin uebergegangen, kochen, 2. Frakt.;

Reference yield: 96.0%

Chloro(chloromethyl)dimethylsilane (1719-57-9) + N-(2-trimethylsiloxyethyl)hexamethyldisilazane (5630-81-9) → chloro-trimethyl-silane (75-77-4) + N,N-bis<(chloromethyl)dimethylsilyl>-2-(trimethylsiloxy)ethylamine

Guidance literature:

With tin(IV) chloride;

upstream raw materials:

trimethylsilyl trifluoromethanesulfonate

2-(trimethylsiloxy)-N-(trimethylsilyl)ethylamine

Downstream raw materials:

chloro-trimethyl-silane

N-<(chloromethyl)dimethylsilyl>-2-(trimethylsiloxy)-N-(trimethylsilyl)ethylamine