2-(3,4-Dimethoxyphenyl)ethyl acetate

Base Information

• Chemical Name: 2-(3,4-Dimethoxyphenyl)ethyl acetate
• CAS No.: 14617-41-5
• Molecular Formula: C12H16 O4
• Molecular Weight: 224.257
• NSC Number: 190951
• DSSTox Substance ID: DTXSID20307386
• Nikkaji Number: J607.776E
• Wikidata: Q82054772
• Mol file: 14617-41-5.mol

Synonyms:14617-41-5;2-(3,4-Dimethoxyphenyl)ethyl acetate;3,4-Dimethoxyphenethyl acetate;NSC190951;3,4-Dimethoxyphenethylacetate;DTXSID20307386;LBERRQIUXJLZNB-UHFFFAOYSA-N;NSC-190951;Benzeneethanol,-3,4-dimethoxy, acetate;2-(3,4-Dimethoxyphenyl)ethyl acetate #;acetic acid 2-(3,4-dimethoxyphenyl)-ethyl ester

Chemical Property of 2-(3,4-Dimethoxyphenyl)ethyl acetate

Chemical Property:

• Vapor Pressure: 0.000632mmHg at 25°C
• Boiling Point: 309.6°Cat760mmHg
• Flash Point: 133.3°C
• Density: 1.084g/cm³
• XLogP3: 1.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 6
• Exact Mass: 224.10485899
• Heavy Atom Count: 16
• Complexity: 217

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)OCCC1=CC(=C(C=C1)OC)OC

Technology Process of 2-(3,4-Dimethoxyphenyl)ethyl acetate

There total 5 articles about 2-(3,4-Dimethoxyphenyl)ethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

acetic anhydride (108-24-7) + 2-(3,4-dimethoxyphenyl)ethyl alcohol (7417-21-2) → β-(3,4-Dimethoxy-phenyl)-ethyl-acetat (14617-41-5)

Guidance literature:

With pyridine; Ambient temperature;

DOI:10.1021/jo00098a039

Reference yield:

2-(3,4-dimethoxyphenyl)-ethylamine (120-20-7) + acetic acid (64-19-7,77671-22-8) → β-(3,4-Dimethoxy-phenyl)-ethyl-acetat (14617-41-5)

Guidance literature:

With dihydrogen peroxide; In ethanol; Heating;

Reference yield:

1,2-dimethoxybenzene (91-16-7) + ethene (74-85-1) + mercury(II) diacetate (1600-27-7) → β-(3,4-Dimethoxy-phenyl)-ethyl-acetat (14617-41-5)

Guidance literature:

With tetrafluoroboric acid; In acetic acid;

upstream raw materials:

2-(3,4-dimethoxyphenyl)-ethylamine

acetic acid

acetic anhydride

2-(3,4-dimethoxyphenyl)ethyl alcohol

Downstream raw materials:

2-(3,4-dimethoxyphenyl)ethyl alcohol

Refernces

• 1、 Lakhrissi, Mohamed,Chapleur, Yves. "Dichloromethylenation of Lactones. 6. Efficient Synthesis of Dichloroolefins from Lactones and Acetates Using Triphenylphosphine and Tetrachloromethane". . p. 5752 - 5757. Retrieved 2007/10/02.