N-Acetyloxy-p-nitrobenzamide

Base Information

Chemical Name:N-Acetyloxy-p-nitrobenzamide
CAS No.:1613-81-6
Molecular Formula:C9H8 N2 O5
Molecular Weight:224.17
Hs Code.:
Mol file:1613-81-6.mol

Synonyms:Benzamide,N-(acetyloxy)-4-nitro- (9CI); Hydroxylamine, O-acetyl-N-(p-nitrobenzoyl)-(7CI,8CI); O-Acetyl-p-nitrobenzohydroxamic acid

Suppliers and Price of N-Acetyloxy-p-nitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of N-Acetyloxy-p-nitrobenzamide

Chemical Property:

PSA：101.22000
Density:1.387g/cm³
LogP:1.71680

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-Acetyloxy-p-nitrobenzamide

There total 10 articles about N-Acetyloxy-p-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 3240-34-4
[bis(acetoxy)iodo]benzene

: 1129-37-9,174848-02-3,20707-69-1
4-nitrobenzaldehyde oxime

: 1613-81-6
O-acetyl-4-nitrobenzohydroxamic acid

Guidance literature:: In acetonitrile; at 20 - 60 ℃; for 2.16667h;
DOI:10.1039/b917096k

Reference yield: 51.0%

: 122-04-3
4-nitro-benzoyl chloride

: 75-36-5
acetyl chloride

: 1613-81-6
O-acetyl-4-nitrobenzohydroxamic acid

Guidance literature:: 4-nitro-benzoyl chloride; With sodium hydroxide; hydroxylamine hydrochloride; In tetrahydrofuran; water; at 20 ℃; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; water;

acetyl chloride; With triethylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol8009682

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 1613-81-6
O-acetyl-4-nitrobenzohydroxamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; sodium hydroxide / water; tetrahydrofuran / 20 °C

2: tetrahydrofuran / 20 °C / Alkaline conditions

With hydroxylamine hydrochloride; sodium hydroxide; In tetrahydrofuran; water;
DOI:10.1039/c4ob00512k