CYCLOPENTYL 4-METHOXYPHENYL KETONE

Base Information

• Chemical Name: CYCLOPENTYL 4-METHOXYPHENYL KETONE
• CAS No.: 15831-52-4
• Molecular Formula: C13H16 O2
• Molecular Weight: 204.269
• Hs Code.: 2914509090
• Mol file: 15831-52-4.mol

Synonyms:Ketone,cyclopentyl p-methoxyphenyl (8CI); Cyclopentyl p-methoxyphenyl ketone; NSC71212; p-Anisyl cyclopentyl ketone

Chemical Property of CYCLOPENTYL 4-METHOXYPHENYL KETONE

Chemical Property:

• Vapor Pressure: 0.000111mmHg at 25°C
• Melting Point: 61-63 °C
• Boiling Point: 336.6°Cat760mmHg
• Flash Point: 150.6°C
• PSA: 26.30000
• Density: 1.076g/cm³
• LogP: 3.06810

Purity/Quality:

99% ^*data from raw suppliers

Cyclopentyl4-methoxyphenylketone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CYCLOPENTYL 4-METHOXYPHENYL KETONE

There total 19 articles about CYCLOPENTYL 4-METHOXYPHENYL KETONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

cyclopentanecarboxylic acid (3400-45-1) + methoxybenzene (100-66-3) → cyclopentyl(4-methoxyphenyl)methanone (15831-52-4)

Guidance literature:

With trifluoroacetic acid; trifluoroacetic anhydride; at 20 ℃;

DOI:10.1002/anie.202105285

Reference yield: 93.0%

4-methoxy-benzaldehyde (123-11-5) + cyclopentene (142-29-0) → cyclopentyl(4-methoxyphenyl)methanone (15831-52-4)

Guidance literature:

(1,2,3,4-Me₄-5-CF₃-cyclopentadiene)Rh(CH₂=CH-SiMe₃)2; In toluene; at 75 ℃; for 2h;

DOI:10.1021/ja066509x

Reference yield: 81.0%

Cyclopentane (287-92-3) + 4-methoxy-benzoyl chloride (100-07-2) → cyclopentyl(4-methoxyphenyl)methanone (15831-52-4)

Guidance literature:

With 2,6-dimethylpyridine; tetrakis(tetrabutylammonium)decatungstate(VI); 4,4'-di-tert-butyl-2,2'-bipyridine nickel(II) bromide; In acetonitrile; at 20 ℃; Inert atmosphere; Irradiation;

DOI:10.1002/anie.202108987

upstream raw materials:

Cyclopentanecarboxylic acid chloride

methoxybenzene

4-methoxybenzonitrile

cyclopentylmagnesium bromide

Downstream raw materials:

4-(1-cyclopentyl-2-phenyl-vinyl)-anisole

Bis-(4-methoxy-phenyl)-cyclopentyliden-methan

Bis-(4-acetoxy-phenyl)-cyclopentyliden-methan

1,1-bis(4-hydroxyphenyl)methylenecyclopentane

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