2,3-DIMETHYLANILINE HYDROCHLORIDE

Base Information

• Chemical Name: 2,3-DIMETHYLANILINE HYDROCHLORIDE
• CAS No.: 5417-45-8
• Molecular Formula: C8H11N
• Molecular Weight: 157.643
• Hs Code.: 2921430090
• Mol file: 5417-45-8.mol

Synonyms:2,3-dimethyl-aniline,hydrochloride;2,3-Dimethylaniline Hydrochloride;2,3-Xylidine Hydrochloride;2,3-Dimethyl-anilin,Hydrochlorid;Dimethylanilin hydrochloride;2,3-dimethylanilinium chloride;dimethylanilinium chloride;

Chemical Property of 2,3-DIMETHYLANILINE HYDROCHLORIDE

Chemical Property:

• Vapor Pressure: 0.00969mmHg at 25°C
• Melting Point: < -15oC
• Boiling Point: 423.8°Cat760mmHg
• Flash Point: 210.1°C
• PSA: 26.02000
• Density: 1.46g/cm³
• LogP: 3.26880
• Water Solubility.: very faint turbidity

Purity/Quality:

98% ^*data from raw suppliers

2,3-Dimethylaniline Hydrochloride ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2,3-Dimethylaniline HCl

Technology Process of 2,3-DIMETHYLANILINE HYDROCHLORIDE

There total 1 articles about 2,3-DIMETHYLANILINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

1-(4-chlorophenyl)-2-methyl-2-propanol (5468-97-3) + α-bromopropionyl bromide (563-76-8) → 2-bromopropanoic acid 1-(4-chlorophenyl)-2-methyl-2-propylester (57469-87-1) + 2,3-dimethylaniline hydrochloride (5417-45-8)

Guidance literature:

With 2,3-Dimethylaniline; In water;

Reference yield: 53.0%

2-amino-4-fluoro-5-iodo-benzoic acid (231278-08-3) + 2,3-dimethylaniline hydrochloride (5417-45-8) + propionic acid anhydride (123-62-6) → 3-(2,3-dimethylphenyl)-2-ethyl-7-fluoro-6-iodoquinazolin-4(3H)-one

Guidance literature:

2-amino-4-fluoro-5-iodo-benzoic acid; propionic acid anhydride; With pyridine; at 0 - 20 ℃; for 0.166667h;

2,3-dimethylaniline hydrochloride; With triphenyl phosphite; for 0.666667h; Microwave irradiation;

Reference yield: 41.1%

butanedial (638-37-9) + 2,3-dimethylaniline hydrochloride (5417-45-8) + 1-(2-chloro-5-pyridylmethyl)-2-nitromethyleneimidazolidine (934236-05-2) → 1-((6-chloropyridin-3-yl)methyl)-10-(2,3-dimethylphenyl)-9-nitro-2,3,5,6,7,8-hexahydro-1H-5,8-epiminoimidazo[1,2-a]azepine

Guidance literature:

In acetonitrile; at 0 ℃; for 1.5h;

DOI:10.1021/jf504014y

upstream raw materials:

1-(4-chlorophenyl)-2-methyl-2-propanol

α-bromopropionyl bromide

Downstream raw materials:

1-isothiocyanato-2,3-dimethylbenzene

1-(2,3-dimethylphenyl)thiourea

Refernces