1-Diphenylamino-2-propanol

Base Information

Chemical Name:1-Diphenylamino-2-propanol
CAS No.:24721-04-8
Molecular Formula:C15H17 N O
Molecular Weight:227.3016
Hs Code.:
NSC Number:106884
Nikkaji Number:J87.462K
Mol file:24721-04-8.mol

Synonyms:24721-04-8;1-Diphenylamino-2-propanol;2-Propanol, 1-diphenylamino-;NSC106884;NSC 106884;BRN 2843569;SCHEMBL5928289;NSC-106884

Suppliers and Price of 1-Diphenylamino-2-propanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-Diphenylamino-2-propanol

Chemical Property:

Vapor Pressure:3.5E-06mmHg at 25°C
Boiling Point:371.7°Cat760mmHg
Flash Point:184°C
Density:1.109g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:227.131014166
Heavy Atom Count:17
Complexity:189

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(CN(C1=CC=CC=C1)C2=CC=CC=C2)O

Technology Process of 1-Diphenylamino-2-propanol

There total 4 articles about 1-Diphenylamino-2-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 65178-51-0
N-allyldiphenylamine

: 24721-04-8
1-(diphenylamino)propan-2-ol

Guidance literature:: With iron(III)-acetylacetonate; methyl 4-nitrobenzenesulfonate; phenylsilane; sodium hydrogencarbonate; In methanol; at 0 - 20 ℃; for 12h; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.202015740

Reference yield: 66.0%

: 74-96-4
ethyl bromide

: 74-97-5
chlorobromomethane

: 1523440-95-0
2-(4-(diphenylamino)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 24721-04-8
1-(diphenylamino)propan-2-ol

Guidance literature:: chlorobromomethane; 2-(4-(diphenylamino)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane); With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h; Schlenk technique; Inert atmosphere; Sealed tube;

With magnesium bromide; In tetrahydrofuran; at 20 ℃; for 1h; Schlenk technique; Inert atmosphere; Sealed tube;

ethyl bromide; Further stages;
DOI:10.1021/jacs.1c06186

Reference yield:

: 122-39-4
diphenylamine

: 24721-04-8
1-(diphenylamino)propan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / 24 h / 120 °C

2.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Schlenk technique; Inert atmosphere; Sealed tube

2.2: 1 h / 20 °C / Schlenk technique; Inert atmosphere; Sealed tube

With n-butyllithium; triethylamine; In tetrahydrofuran;
DOI:10.1021/jacs.1c06186