2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-7H-purin-7-yl)ethyl thiocyanate

Base Information

• Chemical Name: 2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-7H-purin-7-yl)ethyl thiocyanate
• CAS No.: 3737-44-8
• Molecular Formula: C10H11N5O2S
• Molecular Weight: 265.2916
• Mol file: 3737-44-8.mol

Synonyms:

Chemical Property of 2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-7H-purin-7-yl)ethyl thiocyanate

Chemical Property:

• Vapor Pressure: 6.29E-12mmHg at 25°C
• Boiling Point: 544.8°C at 760 mmHg
• Flash Point: 283.3°C
• Density: 1.49g/cm³

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-7H-purin-7-yl)ethyl thiocyanate

There total 3 articles about 2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-7H-purin-7-yl)ethyl thiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

7-(2-hydroxyethyl)theophylline (519-37-9) + potassium thioacyanate (333-20-0) → 1,3-dimethyl-7-(2-thiocyanatoethyl)-1H-purine-2,6(3H,7H)-dione (3737-44-8)

Guidance literature:

With triethylamine; N-tosylimidazole; In N,N-dimethyl-formamide; at 70 ℃; for 7h;

DOI:10.3184/174751916X14736925997854

Reference yield:

7-(2-bromoethyl)-1,3-dimethyl-3,7-dihydro-1H-purin-2,6-dione (23146-05-6) + potassium thioacyanate (333-20-0) → 1,3-dimethyl-7-(2-thiocyanatoethyl)-1H-purine-2,6(3H,7H)-dione (3737-44-8)

Guidance literature:

With acetone;

Reference yield:

→ 1,3-dimethyl-7-(2-thiocyanatoethyl)-1H-purine-2,6(3H,7H)-dione (3737-44-8)

Guidance literature:

7-(2-Brom-aethyl)-theophyllin, KSCN, Butanon, 120grad;

upstream raw materials:

7-(2-bromoethyl)-1,3-dimethyl-3,7-dihydro-1H-purin-2,6-dione

potassium thioacyanate

7-(2-hydroxyethyl)theophylline

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 3737-44-8 2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-7H-purin-7-yl)ethyl thiocyanate

Send

Send

Metric Ton KG G Pound L ML

Send

Send