Bicyclo[2.2.2]octane-1,4-diol 1-acetate

Base Information

• Chemical Name: Bicyclo[2.2.2]octane-1,4-diol 1-acetate
• CAS No.: 54774-94-6
• Molecular Formula: C10H16O3
• Molecular Weight: 184.235
• Mol file: 54774-94-6.mol

Synonyms:Acetic acid 4-hydroxy-bicyclo[2.2.2]oct-1-yl ester;4-Acetoxy-bicyclo<2.2.2>octan-1-ol;4-acetoxybicyclo[2.2.2]octan-1-ol;

Chemical Property of Bicyclo[2.2.2]octane-1,4-diol 1-acetate

Chemical Property:

• Vapor Pressure: 0.0022mmHg at 25°C
• Boiling Point: 257.2°C at 760 mmHg
• Flash Point: 102.7°C
• PSA: 46.53000
• Density: 1.16g/cm³
• LogP: 1.38720

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bicyclo[2.2.2]octane-1,4-diol 1-acetate

There total 18 articles about Bicyclo[2.2.2]octane-1,4-diol 1-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.5%

1,4-Diacetoxybicyclo<2.2.2>octane (10364-35-9) → 4-acetoxybicyclo<2.2.2>octan-1-ol (54774-94-6)

Guidance literature:

With sodium ethanolate; Heating; 1) diethyl ether, reflux, 0.5 h ; 2) benzene, reflux, 3 h;

Reference yield: 48.0%

1,4-dihydroxybicyclo[2.2.2]octane (1194-44-1) + acetic anhydride (108-24-7) → 4-acetoxybicyclo<2.2.2>octan-1-ol (54774-94-6)

Guidance literature:

for 0.583333h; Heating; 1) room temp., 30 min; 2) reflux, 5 min;

Reference yield:

1,4-dimethylidenecyclohexane (4982-20-1) + acetic acid (64-19-7,77671-22-8) → 4-acetoxybicyclo<2.2.2>octan-1-ol (54774-94-6) + 1,4-Diacetoxybicyclo<2.2.2>octane (10364-35-9)

Guidance literature:

With [bis(acetoxy)iodo]benzene; palladium diacetate; In dimethyl sulfoxide; at 20 ℃; Reagent/catalyst;

upstream raw materials:

4-Acetyl-bicyclo<2.2.2>octan-1-ol

1,4-Diacetoxybicyclo<2.2.2>octane

4-Acetoxy-bicyclo<2.2.2>oct-1-yl-p-nitrobenzolsulfonat

1,4-dihydroxybicyclo[2.2.2]octane

Downstream raw materials:

1,4-Dichloro-bicyclo<2.2.2>octane

bicyclo[2.2.2]octane-1,4-dibromide

1,4-diiodobicyclo<2.2.2>octane

bicyclo[2,2,2]octane

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