1-Benzoyl-3-chloro-2-azepanone

Base Information

Chemical Name:1-Benzoyl-3-chloro-2-azepanone
CAS No.:26536-94-7
Molecular Formula:C₁₃H₁₄ClNO₂
Molecular Weight:251.713
Hs Code.:
NSC Number:135375
ChEMBL ID:CHEMBL1350216

Synonyms:1-benzoyl-3-chloroazepan-2-one;1-Benzoyl-3-chloro-2-azepanone;26536-94-7;NSC135375;NSC 135375;3-chloro-1-(phenylcarbonyl)azepan-2-one;2H-Azepin-2-one, 1-benzoyl-3-chlorohexahydro-;MLS001018974;SCHEMBL8778504;CHEMBL1350216;FCTCNPMPXQXJOV-UHFFFAOYSA-N;1-benzoyl-3-chloro-azepan-2-one;HMS2671O12;BBL028586;STK332567;AKOS000266884;AKOS016038911;NSC-135375;NCGC00246055-01;N-benzoyl-alpha-chloro-epsilon-caprolactam;SMR000363382;VS-08857;CS-0358091;SR-01000008849;SR-01000008849-1;Z56885262;F0745-0466

Suppliers and Price of 1-Benzoyl-3-chloro-2-azepanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-Benzoyl-3-chloro-2-azepanone

Chemical Property:

Vapor Pressure:6.32E-07mmHg at 25°C
Boiling Point:409.8°C at 760 mmHg
Flash Point:201.6°C
Density:1.26g/cm³
XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:251.0713064
Heavy Atom Count:17
Complexity:300

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCN(C(=O)C(C1)Cl)C(=O)C2=CC=CC=C2

Technology Process of 1-Benzoyl-3-chloro-2-azepanone

There total 5 articles about 1-Benzoyl-3-chloro-2-azepanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105-60-2,9012-16-2
caprolactam

: 26536-94-7
1-benzoyl-3-chloro-hexahydro-azepin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-aniline

2: tetrachloromethane; chlorine

With tetrachloromethane; chlorine; N,N-dimethyl-aniline;

Reference yield:

: 1709-14-4
α,α-dichlorocaprolactam

: 26536-94-7
1-benzoyl-3-chloro-hexahydro-azepin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; palladium/charcoal; sodium acetate

2: pyridine

With pyridine; palladium on activated charcoal; sodium acetate; acetic acid;
DOI:10.1021/ja01556a019