Benzene, 1-(dimethoxymethyl)-4-methyl-

Base Information

• Chemical Name: Benzene, 1-(dimethoxymethyl)-4-methyl-
• CAS No.: 3395-83-3
• Molecular Formula: C10H14 O2
• Molecular Weight: 166.22
• European Community (EC) Number: 222-244-9
• DSSTox Substance ID: DTXSID7063009
• Nikkaji Number: J183.677C
• Wikidata: Q63409691
• Mol file: 3395-83-3.mol

Synonyms:1-(dimethoxymethyl)-4-methylbenzene;3395-83-3;p-(Dimethoxymethyl)toluene;Benzene, 1-(dimethoxymethyl)-4-methyl-;EINECS 222-244-9;Benzene, 1-methyl-4-(dimethoxymethyl)-;4-(Dimethoxymethyl)toluene;SCHEMBL2431139;DTXSID7063009;p-methylbenzaldehyde dimethylacetal;P-TOLUALDEHYDE DIMETHYLACETAL;CS-0101971;D76271;Q63409691

Chemical Property of Benzene, 1-(dimethoxymethyl)-4-methyl-

Chemical Property:

• Vapor Pressure: 0.567mmHg at 25°C
• Boiling Point: 196.2°Cat760mmHg
• Flash Point: 58.4°C
• PSA: 18.46000
• Density: 0.986g/cm³
• LogP: 2.28640
• XLogP3: 1.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 166.099379685
• Heavy Atom Count: 12
• Complexity: 113

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)C(OC)OC

Technology Process of Benzene, 1-(dimethoxymethyl)-4-methyl-

There total 27 articles about Benzene, 1-(dimethoxymethyl)-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

methanol (67-56-1) + 4-methyl-benzaldehyde (104-87-0) → 4-methylbenzaldehyde dimethylacetal (3395-83-3)

Guidance literature:

Ce⁽³⁺⁾-mont; at 25 ℃; for 12h;

DOI:10.1021/jo00118a021

Reference yield: 95.0%

4-methyl-benzaldehyde (104-87-0) + trimethyl orthoformate (149-73-5) → 4-methylbenzaldehyde dimethylacetal (3395-83-3)

Guidance literature:

With HBF₄*SiO₂; at 25 - 30 ℃; for 0.25h;

DOI:10.1055/s-2008-1042940

Reference yield: 91.6%

methanol (67-56-1) + 4-methyl-benzaldehyde (104-87-0) → 4-methyl-benzoic acid methyl ester (99-75-2) + 4-methylbenzaldehyde dimethylacetal (3395-83-3)

Guidance literature:

With oxygen; Pd₅-Bi₂-Fe₁/⁽¹⁰⁰⁾SiO₂-MgO;

upstream raw materials:

dimethylsulfite

4-methyl-benzaldehyde

methanol

para-xylene

Downstream raw materials:

(α-chloro-4-methyl-benzyl)-methyl ether

N-(methoxy-p-tolyl-methyl)-4-methyl-thiobenzamide

1-methyl-4-(trimethoxymethyl)benzene

4-(methoxymethyl)benzaldehyde