4-AMINO-2-NITROPHENETOLE

Base Information

• Chemical Name: 4-AMINO-2-NITROPHENETOLE
• CAS No.: 1777-87-3
• Molecular Formula: C8H10N2O3
• Molecular Weight: 182.179
• Hs Code.: 2922299090
• Mol file: 1777-87-3.mol

Synonyms:4-ethoxy-3-nitro-aniline;4-Amino-2-nitrophenetole;2-Nitro-4-amino-phenol-aethylaether;2-Nitro-4-amino-phenetol;3-Nitro-p-phenetidin;Benzenamine, 4-ethoxy-3-nitro-;4-Aethoxy-3-nitro-anilin;3-Nitro-p-phenetidine;4-ethoxy-3-nitro-benzenamine;

Chemical Property of 4-AMINO-2-NITROPHENETOLE

Chemical Property:

• Vapor Pressure: 1.87E-05mmHg at 25°C
• Boiling Point: 362.9°C at 760 mmHg
• Flash Point: 173.3°C
• PSA: 81.07000
• Density: 1.264g/cm³
• LogP: 2.68010

Purity/Quality:

97% ^*data from raw suppliers

4-Ethoxy-3-nitroaniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-AMINO-2-NITROPHENETOLE

There total 8 articles about 4-AMINO-2-NITROPHENETOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

2,4-dinitro-1-ethoxybenzene (610-54-8) → 2-Amino-4-nitroethoxybenzen (136-79-8) + 4-ethoxy-3-nitroaniline (1777-87-3)

Guidance literature:

With baker's yeast; In ethanol; water; at 32 ℃; for 96h;

DOI:10.1016/0040-4039(94)80139-8

Reference yield:

ethanol (64-17-5) + 2,4-dinitro-1-ethoxybenzene (610-54-8) → 2-Amino-4-nitroethoxybenzen (136-79-8) + 4-ethoxy-3-nitroaniline (1777-87-3)

Guidance literature:

at 70 ℃;

Reference yield:

4-ethoxyacetanilide (62-44-2,105931-34-8) → 4-ethoxy-3-nitroaniline (1777-87-3)

Guidance literature:

Multi-step reaction with 2 steps

1: HNO₃+H₂SO₄

2: sulfuric acid

With sulfuric acid; nitric acid;

upstream raw materials:

4-ethoxyacetanilide

2,4-dinitro-1-ethoxybenzene

4-ethoxy-3-nitroacetanilide

4-fluoro-2-nitro-phenetole

Downstream raw materials:

4-iodo-2-nitro-phenetole

(2,4-Dinitro-naphthalen-1-yl)-(4-ethoxy-3-nitro-phenyl)-amine

3,3'-dinitrobenzidine