3-Methyl-3-phenylnaphtho(1,2-c)furan-1(3H)-one

Base Information

Chemical Name:3-Methyl-3-phenylnaphtho(1,2-c)furan-1(3H)-one
CAS No.:81194-76-5
Molecular Formula:C19H14O2
Molecular Weight:274.319
Hs Code.:
NSC Number:171723

Synonyms:NSC171723;81194-76-5;NSC 171723;3-Methyl-3-phenylnaphtho(1,2-c)furan-1(3H)-one;3-Methyl-3-phenylnaphtho[1,2-c]furan-1(3H)-one;NSC-171723;3-methyl-3-phenyl-benzo[g]isobenzofuran-1-one

Suppliers and Price of 3-Methyl-3-phenylnaphtho(1,2-c)furan-1(3H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3-Methyl-3-phenylnaphtho(1,2-c)furan-1(3H)-one

Chemical Property:

Vapor Pressure:2.63E-09mmHg at 25°C
Boiling Point:478.2°C at 760 mmHg
Flash Point:202.5°C
Density:1.231g/cm³
XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:274.099379685
Heavy Atom Count:21
Complexity:412

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(C2=C(C3=CC=CC=C3C=C2)C(=O)O1)C4=CC=CC=C4

Technology Process of 3-Methyl-3-phenylnaphtho(1,2-c)furan-1(3H)-one

There total 3 articles about 3-Methyl-3-phenylnaphtho(1,2-c)furan-1(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 917-64-6
methyl magnesium iodide

: 38119-11-8
1-naphthalene carboxylic acid, 2-benzoyl-

: 81194-76-5
3-methyl-3-phenyl-3H-naphtho[1,2-c]furan-1-one

Guidance literature:: With diethyl ether; benzene; anschliessend Ansaeuern;
DOI:10.1021/ja01303a006

Reference yield:

: 879-18-5
naphthalene-1-carbonic acid chloride

: 81194-76-5
3-methyl-3-phenyl-3H-naphtho[1,2-c]furan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 18.5 g / diethyl ether / 1 h / 0 °C

2: 1.) TMEDA, triphenylmethyl chloride, sec-BuLi / 1.) ether, cyclohexane, -78 deg C, 1 h, 2.) a) -78 deg C, 1 h, b) room temp., 3 h

With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; trityl chloride; In diethyl ether;
DOI:10.1021/jo00132a026

Reference yield:

: 5454-10-4
N,N-diethyl-1-naphthamide

: 98-86-2
acetophenone

: 81194-76-5
3-methyl-3-phenyl-3H-naphtho[1,2-c]furan-1-one

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; trityl chloride; Yield given. Multistep reaction; 1.) ether, cyclohexane, -78 deg C, 1 h, 2.) a) -78 deg C, 1 h, b) room temp., 3 h;
DOI:10.1021/jo00132a026