1-Nitrosoadamantane

Base Information

• Chemical Name: 1-Nitrosoadamantane
• CAS No.: 22734-10-7
• Molecular Formula: C10H15NO
• Molecular Weight: 165.235
• Hs Code.: 2904209090
• DSSTox Substance ID: DTXSID50177271
• Nikkaji Number: J543.346K
• Wikidata: Q83047586
• Mol file: 22734-10-7.mol

Synonyms:1-nitrosoadamantane

Chemical Property of 1-Nitrosoadamantane

Chemical Property:

• Vapor Pressure: 0.112mmHg at 25°C
• Refractive Index: 1.717
• Boiling Point: 228.2 °C at 760 mmHg
• Flash Point: 88.6 °C
• PSA: 29.43000
• Density: 1.43 g/cm³
• LogP: 2.72160
• XLogP3: 2.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 165.115364102
• Heavy Atom Count: 12
• Complexity: 183

Purity/Quality:

97% ^*data from raw suppliers

1-NITROSOADAMANTANE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1C2CC3CC1CC(C2)(C3)N=O

Technology Process of 1-Nitrosoadamantane

There total 10 articles about 1-Nitrosoadamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-Adamantanamine (768-94-5) → 1-Nitrosoadamantane (22734-10-7)

Guidance literature:

With peracetic acid; In water; ethyl acetate; at 0 ℃;

DOI:10.1016/S0040-4039(00)99919-2

Reference yield: 36.6%

1-Adamantanamine (768-94-5) → 1-Nitrosoadamantane (22734-10-7) + N,N'-dioxo-1,1'-azobis(adamantane)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In diethyl ether; water; ethyl acetate; for 1h;

DOI:10.1021/ja00147a007

Reference yield:

adamantane (281-23-2) → 1-adamanthanol (768-95-6) + 1-nitroadamantane (7575-82-8) + 1-Nitrosoadamantane (22734-10-7) + 1-nitroxyadamantane (32314-61-7)

Guidance literature:

With dinitrogen pentoxide; In tetrachloromethane; at 15 - 20 ℃; for 1h; Reagent/catalyst;

DOI:10.1134/S107042802010005X

upstream raw materials:

1-nitroadamantane

tert-butylmagnesium chloride

N-adamantylhydroxylamine

1-Adamantanamine

Downstream raw materials:

N-[(3s,5s,7s)-adamantan-1-yl]-N-phenylhydroxylamine

N-(Phenylmethylene)tricyclo<3.3.1.1^3,7>decan-1-amine N-Oxide

N-(1-adamantyl)acetamide

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