DIBENZ(b,f)(1,4)OXAZEPINE, 11-METHYL-

Base Information

Chemical Name:DIBENZ(b,f)(1,4)OXAZEPINE, 11-METHYL-
CAS No.:2868-49-7
Molecular Formula:C₁₄H₁₁NO
Molecular Weight:209.247
Hs Code.:2934999090
DSSTox Substance ID:DTXSID00182835
Nikkaji Number:J42.216I
ChEMBL ID:CHEMBL1256342
Mol file:2868-49-7.mol

Synonyms:BRN 0517480;DIBENZ(b,f)(1,4)OXAZEPINE, 11-METHYL-;2868-49-7;11-Methyldibenz(b,f)(1,4)oxazepine;11-Methyldibenz[b,f][1,4]oxazepine;Dibenz[b,f][1,4]oxazepine, 11-methyl-;11-Methyldibenzo[B,F][1,4]Oxazepine;Oprea1_628777;SCHEMBL1773258;CHEMBL1256342;DTXSID00182835;YOEHNTZDRKGNJG-UHFFFAOYSA-N;AKOS000425322;11-methyl-dibenzo[b,f][1,4]oxazepine;LS-61576

Suppliers and Price of DIBENZ(b,f)(1,4)OXAZEPINE, 11-METHYL-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of DIBENZ(b,f)(1,4)OXAZEPINE, 11-METHYL-

Chemical Property:

Vapor Pressure:0.00124mmHg at 25°C
Boiling Point:308.4°C at 760 mmHg
Flash Point:115.2°C
PSA：21.59000
Density:1.14g/cm³
LogP:3.36860
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:209.084063974
Heavy Atom Count:16
Complexity:287

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NC2=CC=CC=C2OC3=CC=CC=C13

Technology Process of DIBENZ(b,f)(1,4)OXAZEPINE, 11-METHYL-

There total 15 articles about DIBENZ(b,f)(1,4)OXAZEPINE, 11-METHYL- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 143359-96-0
N-(2-phenoxyphenyl)acetamide

: 2868-49-7
(Z)-11-methyldibenzo[b,f][1,4]oxazepine

Guidance literature:: With trichlorophosphate; In dichloromethane; at 120 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c1cc12263k

Reference yield: 86.0%

: 98-86-2
acetophenone

: 95-55-6
2-amino-phenol

: 2868-49-7
(Z)-11-methyldibenzo[b,f][1,4]oxazepine

Guidance literature:: With potassium carbonate; at 100 ℃; for 5h;
DOI:10.1021/acs.orglett.0c02346

Reference yield: 72.0%

: 62469-61-8
11-chloro-dibenz<1,4>oxazepine

: 13170-43-9
(trimethylsilyl)methylmagnesium chloride

: 2868-49-7
(Z)-11-methyldibenzo[b,f][1,4]oxazepine

Guidance literature:: iron(III)-acetylacetonate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; diethyl ether; at 20 ℃; for 0.0833333h;
DOI:10.1021/ol0600234