(5E)-2-mercapto-5-(4-methoxybenzylidene)-3-phenyl-3,5-dihydro-4H-imidazol-4-one

Base Information

• Chemical Name: (5E)-2-mercapto-5-(4-methoxybenzylidene)-3-phenyl-3,5-dihydro-4H-imidazol-4-one
• CAS No.: 101444-70-6
• Molecular Formula: C17H14N2O2S
• Molecular Weight: 310.37000
• Hs Code.: 2933290090
• Mol file: 101444-70-6.mol

Synonyms:5-(4-methoxy-benzylidene)-3-phenyl-2-thioxo-imidazolidin-4-one;5-[(4-methoxyphenyl)methyl]-1,3-thiazole-2-ylamine;2-amino-5-(4-methoxybenzyl)-1,3-thiazole;5-(4-methoxybenzyl)-1,3-thiazol-2-amine;5-(4-methoxybenzyl)thiazol-2-ylamine;5-(4-Methoxy-benzyliden)-3-phenyl-2-thioxo-imidazolidin-4-on;5-(4-methoxybenzyl)thiazol-2-amine;

Chemical Property of (5E)-2-mercapto-5-(4-methoxybenzylidene)-3-phenyl-3,5-dihydro-4H-imidazol-4-one

Chemical Property:

• PSA: 80.70000
• LogP: 2.86930

Purity/Quality:

97% ^*data from raw suppliers

(5E)-2-Mercapto-5-(4-methoxybenzylidene)-3-phenyl-3,5-dihydro-4H-imidazol-4-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: (5E)-2-Mercapto-5-(4-methoxybenzylidene)-3-phenyl-3,5-dihydro-4H-imidazol-4-one is a useful reactant in organic synthesis.

Technology Process of (5E)-2-mercapto-5-(4-methoxybenzylidene)-3-phenyl-3,5-dihydro-4H-imidazol-4-one

There total 2 articles about (5E)-2-mercapto-5-(4-methoxybenzylidene)-3-phenyl-3,5-dihydro-4H-imidazol-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-benzaldehyde (123-11-5) → 5-(4-methoxy-benzylidene)-3-phenyl-2-thioxo-imidazolidin-4-one (101444-70-6)

Guidance literature:

With sodium acetate; acetic acid;

Reference yield:

4-methoxy-benzaldehyde (123-11-5) + phenyl isothiocyanate (103-72-0) + glycine (56-40-6,18875-39-3,25718-94-9) → 5-(4-methoxy-benzylidene)-3-phenyl-2-thioxo-imidazolidin-4-one (101444-70-6)

Guidance literature:

With acetic acid;

Reference yield: 90.0%

2-Mercapto-5-[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-3-phenyl-3,5-dihydro-imidazol-4-one (101444-70-6) + methyl iodide (74-88-4) → 5-(4-methoxybenzylidene)-3-phenyl-2-methylmercaptohydantoin (78283-20-2)

Guidance literature:

With sodium methylate; In methanol;

upstream raw materials:

4-methoxy-benzaldehyde

phenyl isothiocyanate

glycine

Downstream raw materials:

5-(4-methoxybenzylidene)-3-phenyl-2-methylmercaptohydantoin

3-Amino-5-[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-2-[(Z)-phenylimino]-imidazolidin-4-one

2-anilino-5-(4-methoxy-benzylidene)-1,5-dihydro-imidazol-4-one