Benzeneacetic acid, a-(methoxymethylene)-2-(phenylmethoxy)-, methyl ester, (E)-

Base Information

Chemical Name:Benzeneacetic acid, a-(methoxymethylene)-2-(phenylmethoxy)-, methyl ester, (E)-
CAS No.:103497-78-5
Molecular Formula:C18H18O4
Molecular Weight:298.339
Hs Code.:
Mol file:103497-78-5.mol

Synonyms:E-methyl 3-methoxy-2-(2'-benzyloxyphenyl)propenoate;(E)-methyl 2-(2'-benzyloxyphenyl)-3-methoxyacrylate;methyl (E)-2-(2-benzyloxy)phenyl-3-methoxyacrylate;E -methyl 2-(2-benzyloxy)phenyl-3-methoxyacrylate;E-methyl 2-(2-benzyloxy)phenyl-3-methoxyacrylate;

Suppliers and Price of Benzeneacetic acid, a-(methoxymethylene)-2-(phenylmethoxy)-, methyl ester, (E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Benzeneacetic acid, a-(methoxymethylene)-2-(phenylmethoxy)-, methyl ester, (E)-

Chemical Property:

PSA：44.76000
LogP:3.42590

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzeneacetic acid, a-(methoxymethylene)-2-(phenylmethoxy)-, methyl ester, (E)-

There total 14 articles about Benzeneacetic acid, a-(methoxymethylene)-2-(phenylmethoxy)-, methyl ester, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.7%

: 163041-47-2
(Z)-3-methoxy-2-iodo-acrylic acid methyl ester

: 190661-29-1
2-benzyloxyphenylboronic acid

: 103497-78-5
(E)-3-methoxy-2-(2-benzyloxyphenyl)acrylic acid methyl ester

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water; at 90 ℃; for 10h; Solvent; stereoselective reaction; Inert atmosphere;
DOI:10.3184/174751915X14418863197125

Reference yield: 81.0%

: 107-31-3
Methyl formate

: 40525-65-3
2-benzyloxyphenylacetic acid methyl ester

: 103497-78-5
(E)-3-methoxy-2-(2-benzyloxyphenyl)acrylic acid methyl ester

Guidance literature:: Methyl formate; 2-benzyloxyphenylacetic acid methyl ester; With sodium hydride; In N,N-dimethyl-formamide; for 3h;

With potassium carbonate; dimethyl sulfate; In water; N,N-dimethyl-formamide; at 20 ℃; for 2h;