Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-,3'-methanesulfonate

Base Information

Chemical Name:Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-,3'-methanesulfonate
CAS No.:111647-36-0
Molecular Formula:C32H34N2O9S
Molecular Weight:622.696
Hs Code.:

Synonyms:Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-,3'-methanesulfonate

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Chemical Property of Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-,3'-methanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-,3'-methanesulfonate

There total 7 articles about Thymidine, 5'-O-[bis(4-methoxyphenyl)phenylmethyl]-,3'-methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 124-63-0
methanesulfonyl chloride

: 40615-39-2
5'-O-(4-4'-dimethoxytrityl)thymidine

: 111647-36-0
5'-O-(4,4'-dimethoxytrityl)-3'-mesyl-2',3'-dideoxythymidine

Guidance literature:: With pyridine; at 0 ℃; for 5h;
DOI:10.1081/NCN-100107187

Reference yield:

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 111647-36-0
5'-O-(4,4'-dimethoxytrityl)-3'-mesyl-2',3'-dideoxythymidine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 2 h / 20 °C

2: tetrahydrofuran / -8 - 0 °C

With pyridine; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2007.03.086

Reference yield:

: 50-89-5,28854-96-8,3545-96-8,50-88-4
thymidine

: 111647-36-0
5'-O-(4,4'-dimethoxytrityl)-3'-mesyl-2',3'-dideoxythymidine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 2 h / 20 °C

2: tetrahydrofuran / -8 - 0 °C

With pyridine; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2007.03.086