Synonyms:2-(2,5-dimethylphenoxy)ethanol;93-86-7;2-(2,5-Xylyloxy)ethanol;NSC23212;Ethanol,5-xylyloxy)-;SCHEMBL516010;DTXSID40281836;2-(2,5-dimethylphenoxy)ethan-1-ol;NSC-23212;AKOS009560840;A1-05647
99% *data from raw suppliers
There total 6 articles about 2-(2,5-Dimethylphenoxy)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
Reference yield: 93.0%
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The study explores the development of new reactions for constructing five-membered carbocycles, particularly those embedded in polycyclic structures, which are ubiquitous in organic molecules. The authors designed a new type of substrate, 1-ene/yne-VCP, by tethering the two-carbon component to the C(1)-position of vinylcyclopropane (VCP) to achieve a rhodacyclohexene intermediate with a new substitution pattern. The optimized reaction conditions using [Rh(dppp)]SbF6 as the catalyst resulted in high selectivity and yield for the [3 + 2] cycloadducts. Various 1-ene/yne-VCP substrates were tested, yielding moderate to excellent results and demonstrating the versatility of the method. The study also explored the stereoinduction in the [3 + 2] cycloaddition process and extended the reaction to 1-allene-substituted VCP. Control experiments confirmed the crucial role of the vinyl group in the transformation. The proposed mechanism involves the formation of a p-allyl rhodacyclohexene intermediate, followed by insertion and reductive elimination steps.
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